3-[N-(tert-Butyloxycarbonyl)-N-(3-methyl-2-buten-1-yl)]amino-1-benzyloxynaphthalene

Base Information

Chemical Name:3-[N-(tert-Butyloxycarbonyl)-N-(3-methyl-2-buten-1-yl)]amino-1-benzyloxynaphthalene
CAS No.:181574-69-6
Molecular Formula:C₂₇H₃₁NO₃
Molecular Weight:417.548
Hs Code.:

Synonyms:3-[N-(tert-Butyloxycarbonyl)-N-(3-methyl-2-buten-1-yl)]amino-1-benzyloxynaphthalene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-[N-(tert-Butyloxycarbonyl)-N-(3-methyl-2-buten-1-yl)]amino-1-benzyloxynaphthalene

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Technology Process of 3-[N-(tert-Butyloxycarbonyl)-N-(3-methyl-2-buten-1-yl)]amino-1-benzyloxynaphthalene

There total 1 articles about 3-[N-(tert-Butyloxycarbonyl)-N-(3-methyl-2-buten-1-yl)]amino-1-benzyloxynaphthalene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 181574-69-6
3-[N-(tert-Butyloxycarbonyl)-N-(3-methyl-2-buten-1-yl)]amino-1-benzyloxynaphthalene

Guidance literature:

Reference yield:

: Me₂ S

: ethyl acetate n-hexane

: 181574-69-6
3-[N-(tert-Butyloxycarbonyl)-N-(3-methyl-2-buten-1-yl)]amino-1-benzyloxynaphthalene

: 181574-70-9
3-[N-(tert-Butyloxycarbonyl)-N-(formylmethyl)]amino-1-benzyloxynaphthalene

Guidance literature:: With O₃; oxygen; In CH₂ Cl₂ -CH₃ OH;

Reference yield:

: 181574-69-6
3-[N-(tert-Butyloxycarbonyl)-N-(3-methyl-2-buten-1-yl)]amino-1-benzyloxynaphthalene

: 181574-71-0
3-[N-(tert-Butyloxycarbonyl)-N-(3,3-difluoro-2-hydroxy-3-phenylsulfonyl-1-propyl)]amino-1-benzyloxynaphthalene

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) O₃, 2.) Me₂S

2: 51 percent / tetrahydrofuran; hexamethylphosphoric acid triamide / -78 °C

With dimethylsulfide; ozone; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide;
DOI:10.1021/ja961888n