3-[N-(tert-Butyloxycarbonyl)-N-(formylmethyl)]amino-1-benzyloxynaphthalene

Base Information

• Chemical Name: 3-[N-(tert-Butyloxycarbonyl)-N-(formylmethyl)]amino-1-benzyloxynaphthalene
• CAS No.: 181574-70-9
• Molecular Formula: C₂₄H₂₅NO₄
• Molecular Weight: 391.467

Synonyms:3-[N-(tert-Butyloxycarbonyl)-N-(formylmethyl)]amino-1-benzyloxynaphthalene

Chemical Property of 3-[N-(tert-Butyloxycarbonyl)-N-(formylmethyl)]amino-1-benzyloxynaphthalene

Chemical Property:

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Technology Process of 3-[N-(tert-Butyloxycarbonyl)-N-(formylmethyl)]amino-1-benzyloxynaphthalene

There total 3 articles about 3-[N-(tert-Butyloxycarbonyl)-N-(formylmethyl)]amino-1-benzyloxynaphthalene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Me2 S + ethyl acetate n-hexane + 3-[N-(tert-Butyloxycarbonyl)-N-(3-methyl-2-buten-1-yl)]amino-1-benzyloxynaphthalene (181574-69-6) → 3-[N-(tert-Butyloxycarbonyl)-N-(formylmethyl)]amino-1-benzyloxynaphthalene (181574-70-9)

Guidance literature:

With O₃; oxygen; In CH₂ Cl₂ -CH₃ OH;

Reference yield:

N-(tert-butyloxycarbonyl)-4-(benzyloxy)-2-naphthylamine (122745-36-2) → 3-[N-(tert-Butyloxycarbonyl)-N-(formylmethyl)]amino-1-benzyloxynaphthalene (181574-70-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 97 percent / NaH / dimethylformamide / 24 h / 0 - 25 °C

2: 1.) O₃, 2.) Me₂S

With dimethylsulfide; sodium hydride; ozone; In N,N-dimethyl-formamide;

DOI:10.1021/ja961888n

Reference yield:

3-[N-(tert-Butyloxycarbonyl)-N-(3-methyl-2-buten-1-yl)]amino-1-benzyloxynaphthalene (181574-69-6) → 3-[N-(tert-Butyloxycarbonyl)-N-(formylmethyl)]amino-1-benzyloxynaphthalene (181574-70-9)

Guidance literature:

With dimethylsulfide; ozone; Yield given. Multistep reaction;

DOI:10.1021/ja961888n

upstream raw materials:

3-[N-(tert-Butyloxycarbonyl)-N-(3-methyl-2-buten-1-yl)]amino-1-benzyloxynaphthalene

N-(tert-butyloxycarbonyl)-4-(benzyloxy)-2-naphthylamine

Downstream raw materials:

3-[N-(tert-Butyloxycarbonyl)-N-(3,3-difluoro-2-hydroxy-3-phenylsulfonyl-1-propyl)]amino-1-benzyloxynaphthalene

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