N-(p-aminobenzoyl)glycine diazonium salt

Base Information

• Chemical Name: N-(p-aminobenzoyl)glycine diazonium salt
• CAS No.: 82588-16-7
• Molecular Formula: C₉H₈N₃O₃*Cl
• Molecular Weight: 241.634

Synonyms:N-(p-aminobenzoyl)glycine diazonium salt

Chemical Property of N-(p-aminobenzoyl)glycine diazonium salt

Chemical Property:

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Technology Process of N-(p-aminobenzoyl)glycine diazonium salt

There total 1 articles about N-(p-aminobenzoyl)glycine diazonium salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

p-Aminohippuric acid (61-78-9) → N-(p-aminobenzoyl)glycine diazonium salt (82588-16-7)

Guidance literature:

With hydrogenchloride; sodium nitrite; In water; at 0 - 4 ℃; for 1h;

DOI:10.1080/00387010.2010.487508

Reference yield: 48.0%

N-(p-aminobenzoyl)glycine diazonium salt (82588-16-7) + Sodium; 6-methyl-4-oxo-6,7,8,9-tetrahydro-4H-pyrido[1,2-a]pyrimidine-3-carboxylate (32253-86-4) → 9-{[4-(Carboxymethyl-carbamoyl)-phenyl]-hydrazono}-6-methyl-4-oxo-6,7,8,9-tetrahydro-4H-pyrido[1,2-a]pyrimidine-3-carboxylic acid (82588-11-2)

Guidance literature:

With sodium acetate; for 24h;

DOI:10.1021/jm00352a008

Reference yield:

4-Phenylmorpholine (92-53-5) + N-(p-aminobenzoyl)glycine diazonium salt (82588-16-7) → C19H20N4O4

Guidance literature:

In ethanol;

DOI:10.1016/j.bmc.2015.09.015

upstream raw materials:

p-Aminohippuric acid

Downstream raw materials:

9-{[4-(Carboxymethyl-carbamoyl)-phenyl]-hydrazono}-6-methyl-4-oxo-6,7,8,9-tetrahydro-4H-pyrido[1,2-a]pyrimidine-3-carboxylic acid

2-(4-{2-[4-(dimethylamino)phenyl]-1-diazenyl}phenyl)-4-[1-(4-fluorophenyl)methylidene]-1,3-oxazol-5-one

2-(4-{2-[4-(dimethylamino)phenyl]-1-diazenyl}phenyl)-4-{1-[4-(trifluoromethoxy)phenyl]methylidene}-1,3-oxazol-5-one

1-[2-(4-{4-[1-(4-fluorophenyl)methylidene]-5-oxo-4,5-dihydro-1,3-oxazol-2-yl}phenyl)-1-diazenyl]-2-naphthyl acetate

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