dimethyl 3-[4-methoxycarbonyl-2-(4-octadecanoylaminobenzoylamino)phenoxy]phthalate

Base Information

Chemical Name:dimethyl 3-[4-methoxycarbonyl-2-(4-octadecanoylaminobenzoylamino)phenoxy]phthalate
CAS No.:365425-57-6
Molecular Formula:C₄₃H₅₆N₂O₉
Molecular Weight:744.926
Hs Code.:

Synonyms:dimethyl 3-[4-methoxycarbonyl-2-(4-octadecanoylaminobenzoylamino)phenoxy]phthalate

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Chemical Property of dimethyl 3-[4-methoxycarbonyl-2-(4-octadecanoylaminobenzoylamino)phenoxy]phthalate

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Technology Process of dimethyl 3-[4-methoxycarbonyl-2-(4-octadecanoylaminobenzoylamino)phenoxy]phthalate

There total 8 articles about dimethyl 3-[4-methoxycarbonyl-2-(4-octadecanoylaminobenzoylamino)phenoxy]phthalate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 36669-02-0
2,3-bis(methoxycarbonyl)phenol

: 365425-57-6
dimethyl 3-[4-methoxycarbonyl-2-(4-octadecanoylaminobenzoylamino)phenoxy]phthalate

Guidance literature:: Multi-step reaction with 5 steps

1: 86 percent / K₂CO₃ / dimethylformamide / 6 h / 20 °C

2: H₂ / Pd/C / methanol; dioxane / 20 °C / 2280 Torr

3: Et₃N / CHCl₃ / 20 °C

4: H₂ / Pd/C / dioxane; methanol / 20 °C

5: 100 percent / Et₃N / CHCl₃ / 21 h / 20 °C

With hydrogen; potassium carbonate; triethylamine; palladium on activated charcoal; In 1,4-dioxane; methanol; chloroform; N,N-dimethyl-formamide;
DOI:10.1016/S0968-0896(01)00023-2

Reference yield:

: 329-59-9
4-fluoro-3-nitro-benzoic acid methyl ester

: 365425-57-6
dimethyl 3-[4-methoxycarbonyl-2-(4-octadecanoylaminobenzoylamino)phenoxy]phthalate

Guidance literature:: Multi-step reaction with 5 steps

1: 86 percent / K₂CO₃ / dimethylformamide / 6 h / 20 °C

2: H₂ / Pd/C / methanol; dioxane / 20 °C / 2280 Torr

3: Et₃N / CHCl₃ / 20 °C

4: H₂ / Pd/C / dioxane; methanol / 20 °C

5: 100 percent / Et₃N / CHCl₃ / 21 h / 20 °C

With hydrogen; potassium carbonate; triethylamine; palladium on activated charcoal; In 1,4-dioxane; methanol; chloroform; N,N-dimethyl-formamide;
DOI:10.1016/S0968-0896(01)00023-2

Reference yield:

: 122-04-3
4-nitro-benzoyl chloride

: 365425-57-6
dimethyl 3-[4-methoxycarbonyl-2-(4-octadecanoylaminobenzoylamino)phenoxy]phthalate

Guidance literature:: Multi-step reaction with 3 steps

1: Et₃N / CHCl₃ / 20 °C

2: H₂ / Pd/C / dioxane; methanol / 20 °C

3: 100 percent / Et₃N / CHCl₃ / 21 h / 20 °C

With hydrogen; triethylamine; palladium on activated charcoal; In 1,4-dioxane; methanol; chloroform;
DOI:10.1016/S0968-0896(01)00023-2