4-Nitrophenyl N-(5-bromo-2-hydroxybenzyl)-N-methylcarbamate

Base Information

• Chemical Name: 4-Nitrophenyl N-(5-bromo-2-hydroxybenzyl)-N-methylcarbamate
• CAS No.: 309965-24-0
• Molecular Formula: C₁₅H₁₃BrN₂O₅
• Molecular Weight: 381.183
• Mol file: 309965-24-0.mol

Synonyms:4-Nitrophenyl N-(5-bromo-2-hydroxybenzyl)-N-methylcarbamate

Chemical Property of 4-Nitrophenyl N-(5-bromo-2-hydroxybenzyl)-N-methylcarbamate

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of 4-Nitrophenyl N-(5-bromo-2-hydroxybenzyl)-N-methylcarbamate

There total 1 articles about 4-Nitrophenyl N-(5-bromo-2-hydroxybenzyl)-N-methylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

4-Nitrophenyl chloroformate (7693-46-1) + 4-bromo-2-((methylamino)methyl)phenol (157729-23-2) → 4-Nitrophenyl N-(5-bromo-2-hydroxybenzyl)-N-methylcarbamate (309965-24-0)

Guidance literature:

With triethylamine; In diethyl ether; at 20 ℃; for 0.5h;

DOI:10.1135/cccc20001262

Reference yield:

4-Nitrophenyl N-(5-bromo-2-hydroxybenzyl)-N-methylcarbamate (309965-24-0) → 4-nitro-phenol (100-02-7,78813-13-5,89830-32-0) + 6-Bromo-3-methyl-4H-1,3-benzoxazin-2(3H)-one (309965-30-8)

Guidance literature:

With water; In methanol; pH=7.53 - 11.13; Kinetics;

DOI:10.1039/b209323p

upstream raw materials:

4-Nitrophenyl chloroformate

4-bromo-2-((methylamino)methyl)phenol

Downstream raw materials:

4-nitro-phenol

6-Bromo-3-methyl-4H-1,3-benzoxazin-2(3H)-one