5-amino-1-benzyl-4-(N-methoxycarbonylmethyl-N-methyl)carbamoylimidazole

Base Information

Chemical Name:5-amino-1-benzyl-4-(N-methoxycarbonylmethyl-N-methyl)carbamoylimidazole
CAS No.:133124-70-6
Molecular Formula:C₁₅H₁₈N₄O₃
Molecular Weight:302.333
Hs Code.:

Synonyms:5-amino-1-benzyl-4-(N-methoxycarbonylmethyl-N-methyl)carbamoylimidazole

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Chemical Property of 5-amino-1-benzyl-4-(N-methoxycarbonylmethyl-N-methyl)carbamoylimidazole

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Technology Process of 5-amino-1-benzyl-4-(N-methoxycarbonylmethyl-N-methyl)carbamoylimidazole

There total 4 articles about 5-amino-1-benzyl-4-(N-methoxycarbonylmethyl-N-methyl)carbamoylimidazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 133124-69-3
1-benzyl-4-(N-methoxycarbonylmethyl-N-methyl)carbamoyl-5-nitroimidazole

: 133124-70-6
5-amino-1-benzyl-4-(N-methoxycarbonylmethyl-N-methyl)carbamoylimidazole

Guidance literature:: With hydrogen; platinum(IV) oxide; In methanol; for 0.5h; under 2068.6 Torr;

Reference yield:

: 133124-61-5
N-carbonylimidazolyl 1-benzyl-5-nitroimidazole-4-carboxylate

: 133124-70-6
5-amino-1-benzyl-4-(N-methoxycarbonylmethyl-N-methyl)carbamoylimidazole

Guidance literature:: Multi-step reaction with 2 steps

1: 71 percent / tetrahydrofuran; CH₂Cl₂ / 0.5 h / Ambient temperature

2: 60 percent / H₂ / platinum dioxide monohydrate / methanol / 0.5 h / 2068.6 Torr

With hydrogen; platinum(IV) oxide; In tetrahydrofuran; methanol; dichloromethane;

Reference yield:

: 100-44-7
benzyl chloride

: 133124-70-6
5-amino-1-benzyl-4-(N-methoxycarbonylmethyl-N-methyl)carbamoylimidazole

Guidance literature:: Multi-step reaction with 4 steps

1: 1) sodium carbonate, 2) NaOH, KMnO₄ / 1) DMF, 2) water, 36 h

2: 1 h / Heating

3: 71 percent / tetrahydrofuran; CH₂Cl₂ / 0.5 h / Ambient temperature

4: 60 percent / H₂ / platinum dioxide monohydrate / methanol / 0.5 h / 2068.6 Torr

With sodium hydroxide; potassium permanganate; hydrogen; sodium carbonate; platinum(IV) oxide; In tetrahydrofuran; methanol; dichloromethane;