1-benzyl-4-(N-methoxycarbonylmethyl-N-methyl)carbamoyl-5-nitroimidazole

Base Information

Chemical Name:1-benzyl-4-(N-methoxycarbonylmethyl-N-methyl)carbamoyl-5-nitroimidazole
CAS No.:133124-69-3
Molecular Formula:C₁₅H₁₆N₄O₅
Molecular Weight:332.316
Hs Code.:

Synonyms:1-benzyl-4-(N-methoxycarbonylmethyl-N-methyl)carbamoyl-5-nitroimidazole

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Chemical Property of 1-benzyl-4-(N-methoxycarbonylmethyl-N-methyl)carbamoyl-5-nitroimidazole

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Technology Process of 1-benzyl-4-(N-methoxycarbonylmethyl-N-methyl)carbamoyl-5-nitroimidazole

There total 3 articles about 1-benzyl-4-(N-methoxycarbonylmethyl-N-methyl)carbamoyl-5-nitroimidazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 5473-12-1
N-methylglycine methylester

: 133124-61-5
N-carbonylimidazolyl 1-benzyl-5-nitroimidazole-4-carboxylate

: 133124-69-3
1-benzyl-4-(N-methoxycarbonylmethyl-N-methyl)carbamoyl-5-nitroimidazole

Guidance literature:: In tetrahydrofuran; dichloromethane; for 0.5h; Ambient temperature;

Reference yield:

: 100-44-7
benzyl chloride

: 133124-69-3
1-benzyl-4-(N-methoxycarbonylmethyl-N-methyl)carbamoyl-5-nitroimidazole

Guidance literature:: Multi-step reaction with 3 steps

1: 1) sodium carbonate, 2) NaOH, KMnO₄ / 1) DMF, 2) water, 36 h

2: 1 h / Heating

3: 71 percent / tetrahydrofuran; CH₂Cl₂ / 0.5 h / Ambient temperature

With sodium hydroxide; potassium permanganate; sodium carbonate; In tetrahydrofuran; dichloromethane;

Reference yield:

: 69195-96-6
5-nitro-1-(phenylmethyl)-1H-imidazole-4-carboxylic acid

: 133124-69-3
1-benzyl-4-(N-methoxycarbonylmethyl-N-methyl)carbamoyl-5-nitroimidazole

Guidance literature:: Multi-step reaction with 2 steps

1: 1 h / Heating

2: 71 percent / tetrahydrofuran; CH₂Cl₂ / 0.5 h / Ambient temperature

In tetrahydrofuran; dichloromethane;