N-phenyl-C-(2-thienyl)formohydrazidoyl chloride

Base Information

Chemical Name:N-phenyl-C-(2-thienyl)formohydrazidoyl chloride
CAS No.:36756-95-3
Molecular Formula:C₁₁H₉ClN₂S
Molecular Weight:236.725
Hs Code.:

Synonyms:N-phenyl-C-(2-thienyl)formohydrazidoyl chloride

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-phenyl-C-(2-thienyl)formohydrazidoyl chloride

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Technology Process of N-phenyl-C-(2-thienyl)formohydrazidoyl chloride

There total 8 articles about N-phenyl-C-(2-thienyl)formohydrazidoyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 36668-22-1
N′-phenylthiophene-2-carbohydrazide

: 36756-95-3
N-phenyl-C-(2-thienyl)formohydrazidoyl chloride

Guidance literature:: With tetrachloromethane; (C₅H₅)3P; In acetonitrile; for 10h;

Reference yield:

: 36668-22-1
N′-phenylthiophene-2-carbohydrazide

: 36756-95-3
(Z)-N-phenylthiophene-2-carbohydrazonyl chloride

Guidance literature:: With tetrachloromethane; triphenylphosphine; In acetonitrile; at 20 ℃;
DOI:10.1021/acs.orglett.5b03598

Reference yield:

: 5271-67-0
2-Thiophenecarbonyl chloride

: 36756-95-3
N-phenyl-C-(2-thienyl)formohydrazidoyl chloride

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / dichloromethane / 16 h / 0 - 20 °C

2: tetrachloromethane; triphenylphosphine / acetonitrile / 16 h / 20 °C

With pyridine; tetrachloromethane; triphenylphosphine; In dichloromethane; acetonitrile;
DOI:10.1002/anie.202003219