N-[2,6-dimethyl-4-{1-hydroxy-2,2,2-trifluoro-1-(trifluoromethyl)-ethyl}phenyl] 3-aminobenzamide

Base Information

Chemical Name:N-[2,6-dimethyl-4-{1-hydroxy-2,2,2-trifluoro-1-(trifluoromethyl)-ethyl}phenyl] 3-aminobenzamide
CAS No.:914463-27-7
Molecular Formula:C₁₈H₁₆F₆N₂O₂
Molecular Weight:406.328
Hs Code.:

Synonyms:N-[2,6-dimethyl-4-{1-hydroxy-2,2,2-trifluoro-1-(trifluoromethyl)-ethyl}phenyl] 3-aminobenzamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-[2,6-dimethyl-4-{1-hydroxy-2,2,2-trifluoro-1-(trifluoromethyl)-ethyl}phenyl] 3-aminobenzamide

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Technology Process of N-[2,6-dimethyl-4-{1-hydroxy-2,2,2-trifluoro-1-(trifluoromethyl)-ethyl}phenyl] 3-aminobenzamide

There total 2 articles about N-[2,6-dimethyl-4-{1-hydroxy-2,2,2-trifluoro-1-(trifluoromethyl)-ethyl}phenyl] 3-aminobenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 914463-26-6
N-[2,6-dimethyl-4-{1-hydroxy-2,2,2-trifluoro-1-(trifluoromethyl)-ethyl}phenyl] 3-nitrobenzamide

: 914463-27-7
N-[2,6-dimethyl-4-{1-hydroxy-2,2,2-trifluoro-1-(trifluoromethyl)-ethyl}phenyl] 3-aminobenzamide

Guidance literature:: With hydrogen; palladium on activated charcoal; In methanol; at 20 ℃;

Reference yield:

: 87-62-7
2,6-dimethylaniline

: 914463-27-7
N-[2,6-dimethyl-4-{1-hydroxy-2,2,2-trifluoro-1-(trifluoromethyl)-ethyl}phenyl] 3-aminobenzamide

Guidance literature:: Multi-step reaction with 3 steps

1: toluene-4-sulfonic acid / water / 100 °C

2: pyridine / tetrahydrofuran / 20 °C

3: hydrogen / palladium 10% on activated carbon / methanol / 20 °C

With pyridine; hydrogen; toluene-4-sulfonic acid; palladium 10% on activated carbon; In tetrahydrofuran; methanol; water;