undec-10-enoic acid methylphenylamide

Base Information

Chemical Name:undec-10-enoic acid methylphenylamide
CAS No.:76691-54-8
Molecular Formula:C₁₈H₂₇NO
Molecular Weight:273.418
Hs Code.:

Synonyms:undec-10-enoic acid methylphenylamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of undec-10-enoic acid methylphenylamide

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Technology Process of undec-10-enoic acid methylphenylamide

There total 2 articles about undec-10-enoic acid methylphenylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 112-38-9
10-undecenoic acid

: 100-61-8
N-methylaniline

: 76691-54-8
undec-10-enoic acid methylphenylamide

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In dichloromethane; at 0 - 24 ℃; Inert atmosphere;
DOI:10.1002/adsc.200700595

Reference yield:

: 38460-95-6
undec-10-enoyl chloride

: 100-61-8
N-methylaniline

: 76691-54-8
undec-10-enoic acid methylphenylamide

Guidance literature:: With pyridine; benzene;

Reference yield: 96.0%

: 201230-82-2
carbon monoxide

: 76691-54-8
undec-10-enoic acid methylphenylamide

: 295365-33-2
ethyl tert-butoxycarbonylamino(toluene-4-sulfonyl)acetate

: ethyl (2S,3R)-(2-tert-butoxycarbonylamino)-3-formyl-12-(methylphenylcarbamoyl)dodecanoate

Guidance literature:: With (S)-2-{bis[3,5-bis(trifluoromethyl)phenyl][(trimethylsilanyl)oxy]methyl}pyrrolidine; dipotassium hydrogenphosphate; 1,2,3-trimethoxybenzene; dicarbonyl(acetylacotonato)rhodium(I); hydrogen; (2-oxo-1,2-dihydro-6-pyridyl)diphenylphosphine; In chloroform; at 45 ℃; for 24h; under 15001.5 Torr; enantioselective reaction; Autoclave; Inert atmosphere;
DOI:10.1055/s-0033-1338602