N-(2-(2-(4-methoxybenzylamino)-2-oxoethylthio)benzothiazol-6-yl)-4-nitrobenzamide

Base Information

Chemical Name:N-(2-(2-(4-methoxybenzylamino)-2-oxoethylthio)benzothiazol-6-yl)-4-nitrobenzamide
CAS No.:531530-49-1
Molecular Formula:C₂₄H₂₀N₄O₅S₂
Molecular Weight:508.579
Hs Code.:

Synonyms:N-(2-(2-(4-methoxybenzylamino)-2-oxoethylthio)benzothiazol-6-yl)-4-nitrobenzamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(2-(2-(4-methoxybenzylamino)-2-oxoethylthio)benzothiazol-6-yl)-4-nitrobenzamide

Chemical Property:

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Technology Process of N-(2-(2-(4-methoxybenzylamino)-2-oxoethylthio)benzothiazol-6-yl)-4-nitrobenzamide

There total 3 articles about N-(2-(2-(4-methoxybenzylamino)-2-oxoethylthio)benzothiazol-6-yl)-4-nitrobenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 532422-39-2
C₁₇H₁₇N₃O₂S₂

: 122-04-3
4-nitro-benzoyl chloride

: 531530-49-1
N-(2-(2-(4-methoxybenzylamino)-2-oxoethylthio)benzothiazol-6-yl)-4-nitrobenzamide

Guidance literature:: With sodium hydrogencarbonate; In dichloromethane; at 20 ℃; for 12h;
DOI:10.1016/j.bmcl.2010.12.124

Reference yield:

: 2393-23-9
4-methoxy-benzylamine

: 531530-49-1
N-(2-(2-(4-methoxybenzylamino)-2-oxoethylthio)benzothiazol-6-yl)-4-nitrobenzamide

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate / dichloromethane / 0 °C / Reflux

2: potassium carbonate / acetone / 4 h / Reflux

3: sodium hydrogencarbonate / dichloromethane / 12 h / 20 °C

With sodium hydrogencarbonate; potassium carbonate; In dichloromethane; acetone;
DOI:10.1016/j.bmcl.2010.12.124

Reference yield:

: 81494-05-5
2-chloro-N-(4-methoxybenzyl)acetamide

: 531530-49-1
N-(2-(2-(4-methoxybenzylamino)-2-oxoethylthio)benzothiazol-6-yl)-4-nitrobenzamide

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / acetone / 4 h / Reflux

2: sodium hydrogencarbonate / dichloromethane / 12 h / 20 °C

With sodium hydrogencarbonate; potassium carbonate; In dichloromethane; acetone;
DOI:10.1016/j.bmcl.2010.12.124