mesitylfluorenyldimethoxygermane

Base Information

Chemical Name:mesitylfluorenyldimethoxygermane
CAS No.:134691-74-0
Molecular Formula:C₂₄H₂₆GeO₂
Molecular Weight:419.059
Hs Code.:

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Suppliers and Price of mesitylfluorenyldimethoxygermane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of mesitylfluorenyldimethoxygermane

Chemical Property:

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Technology Process of mesitylfluorenyldimethoxygermane

There total 1 articles about mesitylfluorenyldimethoxygermane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 126529-82-6
tris(methoxy)mesitylgermane

: 881-04-9
9H-fluoren-9-yllithium

: 134691-74-0
mesitylfluorenyldimethoxygermane

Guidance literature:: In diethyl ether; byproducts: CH3OLi; (N2 or Ar); addn. of compounds at -78°C; warmed to room temp.; stirred for 1 h at 35°C; filtration; distn. of solvents in vacuo; double recrystn. (pentane);

Reference yield: 71.0%

: 134691-74-0
mesitylfluorenyldimethoxygermane

: 134691-77-3
mesitylfluorenyldichlorogermane

Guidance literature:: With hydrogenchloride; In diethyl ether; byproducts: CH3OH, fluorene; (N2 or Ar); addn. of compounds at -78°C; warmed to room temp.; evapn. in vacuo; fractional crystn. in pentane; filtration;

Reference yield: 58.0%

: 134691-74-0
mesitylfluorenyldimethoxygermane

: 134691-78-4
mesitylfluorenyldifluorogermane

Guidance literature:: With hydrogen fluoride; In tetrahydrofuran; water; byproducts: CH3OH; (N2 or Ar); addn. of compounds at 0°C; warmed to room temp.; filtration; dissolved in THF; dried over Na2SO4; recrystd. at low temp.;