(4S)-3-[(2R,3R)-3-(N-benzoyloxy-N-benzylamino)-2-methyl-3-phenylpropionyl]-4-(1-methylethyl)-2-oxazolidinone

Base Information

Chemical Name:(4S)-3-[(2R,3R)-3-(N-benzoyloxy-N-benzylamino)-2-methyl-3-phenylpropionyl]-4-(1-methylethyl)-2-oxazolidinone
CAS No.:245351-07-9
Molecular Formula:C₃₀H₃₂N₂O₅
Molecular Weight:500.594
Hs Code.:

Synonyms:(4S)-3-[(2R,3R)-3-(N-benzoyloxy-N-benzylamino)-2-methyl-3-phenylpropionyl]-4-(1-methylethyl)-2-oxazolidinone

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Chemical Property of (4S)-3-[(2R,3R)-3-(N-benzoyloxy-N-benzylamino)-2-methyl-3-phenylpropionyl]-4-(1-methylethyl)-2-oxazolidinone

Chemical Property:

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Technology Process of (4S)-3-[(2R,3R)-3-(N-benzoyloxy-N-benzylamino)-2-methyl-3-phenylpropionyl]-4-(1-methylethyl)-2-oxazolidinone

There total 6 articles about (4S)-3-[(2R,3R)-3-(N-benzoyloxy-N-benzylamino)-2-methyl-3-phenylpropionyl]-4-(1-methylethyl)-2-oxazolidinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 77877-19-1,165657-81-8
N-isopropyl oxazolidinone

: N-benzoyloxy-N-benzylidenebenzylammonium chloride

: 245351-07-9
(4S)-3-[(2R,3R)-3-(N-benzoyloxy-N-benzylamino)-2-methyl-3-phenylpropionyl]-4-(1-methylethyl)-2-oxazolidinone

: 245351-06-8
(4S)-3-[(2R,3S)-3-(N-benzoyloxy-N-benzylamino)-2-methyl-3-phenylpropionyl]-4-(1-methylethyl)-2-oxazolidinone

Guidance literature:: N-isopropyl oxazolidinone; With titanium(IV) isopropylate; titanium tetrachloride; N-ethyl-N,N-diisopropylamine; In dichloromethane;

N-benzoyloxy-N-benzylidenebenzylammonium chloride; In dichloromethane; at -78 ℃; for 1h;
DOI:10.1246/bcsj.73.2423

Reference yield:

: 3376-26-9
N-Benzylidenebenzylamine N-oxide

: 245351-07-9
(4S)-3-[(2R,3R)-3-(N-benzoyloxy-N-benzylamino)-2-methyl-3-phenylpropionyl]-4-(1-methylethyl)-2-oxazolidinone

Guidance literature:: Multi-step reaction with 2 steps

1: CH₂Cl₂ / 0.5 h / -70 °C

2: CH₂Cl₂ / 1 h / -78 °C

In dichloromethane;
DOI:10.1246/bcsj.73.2423

Reference yield:

: 98-88-4
benzoyl chloride

: 245351-07-9
(4S)-3-[(2R,3R)-3-(N-benzoyloxy-N-benzylamino)-2-methyl-3-phenylpropionyl]-4-(1-methylethyl)-2-oxazolidinone

Guidance literature:: Multi-step reaction with 2 steps

1: CH₂Cl₂ / 0.5 h / -70 °C

2: CH₂Cl₂ / 1 h / -78 °C

In dichloromethane;
DOI:10.1246/bcsj.73.2423