methyl 1,2,4-tri-O-acetyl-3-O-benzyl-β-L-idopyranosyluronate

Base Information

Chemical Name:methyl 1,2,4-tri-O-acetyl-3-O-benzyl-β-L-idopyranosyluronate
CAS No.:87326-79-2
Molecular Formula:C₂₀H₂₄O₁₀
Molecular Weight:424.405
Hs Code.:

Synonyms:methyl 1,2,4-tri-O-acetyl-3-O-benzyl-β-L-idopyranosyluronate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl 1,2,4-tri-O-acetyl-3-O-benzyl-β-L-idopyranosyluronate

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Technology Process of methyl 1,2,4-tri-O-acetyl-3-O-benzyl-β-L-idopyranosyluronate

There total 14 articles about methyl 1,2,4-tri-O-acetyl-3-O-benzyl-β-L-idopyranosyluronate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 87326-77-0,87326-78-1
methyl 3-O-benzyl-L-idopyranosyluronate

: 75-36-5
acetyl chloride

: 87326-79-2
methyl 1,2,4-tri-O-acetyl-3-O-benzyl-β-L-idopyranosyluronate

Guidance literature:: With pyridine; dmap; In dichloromethane; at -40 ℃; for 10h; Inert atmosphere;
DOI:10.1021/ja4027727

Reference yield: 99.0%

: 1394857-11-4
1,2,4-tri-O-acetyl-3-O-benzyl-β-L-idopyranuronic acid

: 74-88-4
methyl iodide

: 87326-79-2
methyl 1,2,4-tri-O-acetyl-3-O-benzyl-β-L-idopyranosyluronate

Guidance literature:: With potassium hydrogencarbonate; In N,N-dimethyl-formamide; for 24h; Inert atmosphere;
DOI:10.1021/jo300722y

Reference yield: 83.0%

: 87326-78-1
methyl 3-O-benzyl-β-L-idopyranuronate

: 75-36-5
acetyl chloride

: 87326-80-5
methyl 1,2,4-tri-O-acetyl-3-O-benzyl-α-L-idopyranuronate

: 87326-79-2
methyl 1,2,4-tri-O-acetyl-3-O-benzyl-β-L-idopyranosyluronate

Guidance literature:: With pyridine; 2,4-dimethylaminopyridine; In dichloromethane; at -40 ℃; for 10h; Further Variations:; Temperatures; Solvents; Product distribution;
DOI:10.1016/S0008-6215(02)00525-6