Ethyl 7-Methyl-3-oxo-2-(triphenylphosphoranylidene)-(E)-4,6-octadienoate

Base Information

Chemical Name:Ethyl 7-Methyl-3-oxo-2-(triphenylphosphoranylidene)-(E)-4,6-octadienoate
CAS No.:84454-76-2
Molecular Formula:C₂₉H₂₉O₃P
Molecular Weight:456.521
Hs Code.:

Synonyms:Ethyl 7-Methyl-3-oxo-2-(triphenylphosphoranylidene)-(E)-4,6-octadienoate

Suppliers and Price of Ethyl 7-Methyl-3-oxo-2-(triphenylphosphoranylidene)-(E)-4,6-octadienoate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of Ethyl 7-Methyl-3-oxo-2-(triphenylphosphoranylidene)-(E)-4,6-octadienoate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of Ethyl 7-Methyl-3-oxo-2-(triphenylphosphoranylidene)-(E)-4,6-octadienoate

There total 1 articles about Ethyl 7-Methyl-3-oxo-2-(triphenylphosphoranylidene)-(E)-4,6-octadienoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 107-86-8
3,3-dimethyl acrylaldehyde

: 78980-76-4
diethyl <2,4-dioxo-4-ethoxy-3-(triphenylphosphoranylidene)butyl>-phosphonate

: 84454-76-2
Ethyl 7-Methyl-3-oxo-2-(triphenylphosphoranylidene)-(E)-4,6-octadienoate

Guidance literature:: With methanol; sodium hydride; In tetrahydrofuran; at 25 ℃; for 2h;
DOI:10.1021/jo00153a027

Reference yield:

: 84454-76-2
Ethyl 7-Methyl-3-oxo-2-(triphenylphosphoranylidene)-(E)-4,6-octadienoate

: 58191-71-2,61008-99-9,61009-00-5
2,5-Dimethyl-3-vinyl-hex-4-enoic acid

Guidance literature:: Multi-step reaction with 2 steps

2: 4 N NaOH, 0.82 N NaOCl / acetonitrile / 1) 0 degC, 3 h, 2) 20 degC, 3 h

With sodium hydroxide; sodium hypochlorite; In acetonitrile;
DOI:10.1021/jo00153a027