C₇H₆BrFN₂O

Base Information

Chemical Name:C₇H₆BrFN₂O
CAS No.:1616667-62-9
Molecular Formula:C₇H₆BrFN₂O
Molecular Weight:233.04
Hs Code.:

C<sub>7</sub>H<sub>6</sub>BrFN<sub>2</sub>O

Synonyms:C₇H₆BrFN₂O

Suppliers and Price of C₇H₆BrFN₂O

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₇H₆BrFN₂O

Chemical Property:

Purity/Quality:

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Technology Process of C₇H₆BrFN₂O

There total 2 articles about C₇H₆BrFN₂O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 29682-15-3
methyl 5-bromopicolinate

: 74-89-5
methylamine

: 1616667-62-9
C₇H₆BrFN₂O

Guidance literature:: methyl 5-bromopicolinate; With silver(II) fluoride; Inert atmosphere; Glovebox;

methylamine; In methanol; water; at 25 ℃; for 1.5h;

Reference yield:

: 29682-15-3
methyl 5-bromopicolinate

: 1616667-62-9
C₇H₆BrFN₂O

Guidance literature:: Multi-step reaction with 2 steps

1: silver(II) fluoride / acetonitrile / 1 h / 20 °C / Inert atmosphere; Glovebox; Sealed tube

2: water / 1.5 h / 20 °C / Sealed tube

With silver(II) fluoride; In water; acetonitrile;
DOI:10.1021/ja5049303

Reference yield:

: 1616667-62-9
C₇H₆BrFN₂O

: 875051-72-2
[6-amino-5-(2,3,5-trichlorophenyl)pyridine-2-carboxylic acid methylamide]

Guidance literature:: Multi-step reaction with 2 steps

1.1: ammonium hydroxide; potassium carbonate / dimethyl sulfoxide / 12 h / 80 °C / Inert atmosphere; Glovebox; Sealed tube

2.1: tributylphosphine; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; potassium fluoride / tetrahydrofuran; water / 0.03 h / 20 °C

2.2: 3 h / 20 °C

With potassium fluoride; ammonium hydroxide; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; tributylphosphine; potassium carbonate; In tetrahydrofuran; water; dimethyl sulfoxide;
DOI:10.1021/ja5049303