tert-butyl (2S,3S,αS)-2-benzyloxy-3-[N-benzyl-N-(α-methylbenzyl)amino]-4-(tri-iso-propylsilyloxy)butanoate

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Chemical Name:tert-butyl (2S,3S,αS)-2-benzyloxy-3-[N-benzyl-N-(α-methylbenzyl)amino]-4-(tri-iso-propylsilyloxy)butanoate
CAS No.:1033367-38-2
Molecular Formula:C₃₉H₅₇NO₄Si
Molecular Weight:631.971
Hs Code.:

Synonyms:tert-butyl (2S,3S,αS)-2-benzyloxy-3-[N-benzyl-N-(α-methylbenzyl)amino]-4-(tri-iso-propylsilyloxy)butanoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of tert-butyl (2S,3S,αS)-2-benzyloxy-3-[N-benzyl-N-(α-methylbenzyl)amino]-4-(tri-iso-propylsilyloxy)butanoate

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Technology Process of tert-butyl (2S,3S,αS)-2-benzyloxy-3-[N-benzyl-N-(α-methylbenzyl)amino]-4-(tri-iso-propylsilyloxy)butanoate

There total 1 articles about tert-butyl (2S,3S,αS)-2-benzyloxy-3-[N-benzyl-N-(α-methylbenzyl)amino]-4-(tri-iso-propylsilyloxy)butanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 1033129-99-5
tert-butyl (2S,3S,αS)-2-hydroxy-3-[N-benzyl-N-(α-methylbenzyl)amino]-4-tri-iso-propylsilyloxybutanoate

: 100-39-0
benzyl bromide

: 1033367-38-2
tert-butyl (2S,3S,αS)-2-benzyloxy-3-[N-benzyl-N-(α-methylbenzyl)amino]-4-(tri-iso-propylsilyloxy)butanoate

Guidance literature:: tert-butyl (2S,3S,αS)-2-hydroxy-3-[N-benzyl-N-(α-methylbenzyl)amino]-4-tri-iso-propylsilyloxybutanoate; With sodium hydride; In tetrahydrofuran; at 0 - 20 ℃;

benzyl bromide; With 15-crown-5; In tetrahydrofuran; at 20 ℃; for 12h; optical yield given as %de;
DOI:10.1039/b801671b