1-O-p-methoxyphenyl 2,3,4-tri-O-benzoyl-6-O-tert-butyldiphenylsilyl-β-D-glucopyranose

Base Information

Chemical Name:1-O-p-methoxyphenyl 2,3,4-tri-O-benzoyl-6-O-tert-butyldiphenylsilyl-β-D-glucopyranose
CAS No.:1344980-48-8
Molecular Formula:C₅₀H₄₈O₁₀Si
Molecular Weight:837.011
Hs Code.:

Synonyms:1-O-p-methoxyphenyl 2,3,4-tri-O-benzoyl-6-O-tert-butyldiphenylsilyl-β-D-glucopyranose

Suppliers and Price of 1-O-p-methoxyphenyl 2,3,4-tri-O-benzoyl-6-O-tert-butyldiphenylsilyl-β-D-glucopyranose

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-O-p-methoxyphenyl 2,3,4-tri-O-benzoyl-6-O-tert-butyldiphenylsilyl-β-D-glucopyranose

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of 1-O-p-methoxyphenyl 2,3,4-tri-O-benzoyl-6-O-tert-butyldiphenylsilyl-β-D-glucopyranose

There total 6 articles about 1-O-p-methoxyphenyl 2,3,4-tri-O-benzoyl-6-O-tert-butyldiphenylsilyl-β-D-glucopyranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 1075709-09-9
1-O-p-methoxyphenyl 6-O-tert-butyldiphenylsilyl-β-D-glucopyranose

: 98-88-4
benzoyl chloride

: 1344980-48-8
1-O-p-methoxyphenyl 2,3,4-tri-O-benzoyl-6-O-tert-butyldiphenylsilyl-β-D-glucopyranose

Guidance literature:: With pyridine; dmap; for 1h; Inert atmosphere; Cooling with ice;

Reference yield:

: 2872-65-3,14581-81-8,17042-40-9,84380-06-3,105260-62-6
p-methoxyphenyl 2,3,4,6-tetra-O-acetyl-β-D-glucopyranoside

: 1344980-48-8
1-O-p-methoxyphenyl 2,3,4-tri-O-benzoyl-6-O-tert-butyldiphenylsilyl-β-D-glucopyranose

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium methylate / methanol / 2 h / 20 °C / pH 9 - 10

1.2: 13 h / 20 °C / Inert atmosphere; Cooling with ice

2.1: dmap; pyridine / 1 h / Inert atmosphere; Cooling with ice

With pyridine; dmap; sodium methylate; In methanol;

Reference yield:

: 150-76-5
4-methoxy-phenol

: 1344980-48-8
1-O-p-methoxyphenyl 2,3,4-tri-O-benzoyl-6-O-tert-butyldiphenylsilyl-β-D-glucopyranose

Guidance literature:: Multi-step reaction with 3 steps

1.1: boron trifluoride diethyl etherate / dichloromethane / 1 h / Inert atmosphere; Cooling with ice

2.1: sodium methylate / methanol / 2 h / 20 °C / pH 9 - 10

2.2: 13 h / 20 °C / Inert atmosphere; Cooling with ice

3.1: dmap; pyridine / 1 h / Inert atmosphere; Cooling with ice

With pyridine; dmap; boron trifluoride diethyl etherate; sodium methylate; In methanol; dichloromethane;