O₂-(2,4-dinitrophenyl)-1-{[4-(2-(2-hydroxyethoxy))ethyl]piperazin-1-yl}diazen-1-ium-1,2-diolate

Base Information

• Chemical Name: O₂-(2,4-dinitrophenyl)-1-{[4-(2-(2-hydroxyethoxy))ethyl]piperazin-1-yl}diazen-1-ium-1,2-diolate
• CAS No.: 1362738-98-4
• Molecular Formula: C₁₄H₂₀N₆O₈
• Molecular Weight: 400.348

Synonyms:O₂-(2,4-dinitrophenyl)-1-{[4-(2-(2-hydroxyethoxy))ethyl]piperazin-1-yl}diazen-1-ium-1,2-diolate

Chemical Property of O₂-(2,4-dinitrophenyl)-1-{[4-(2-(2-hydroxyethoxy))ethyl]piperazin-1-yl}diazen-1-ium-1,2-diolate

Chemical Property:

Purity/Quality:

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Technology Process of O₂-(2,4-dinitrophenyl)-1-{[4-(2-(2-hydroxyethoxy))ethyl]piperazin-1-yl}diazen-1-ium-1,2-diolate

There total 2 articles about O₂-(2,4-dinitrophenyl)-1-{[4-(2-(2-hydroxyethoxy))ethyl]piperazin-1-yl}diazen-1-ium-1,2-diolate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

sodium [1-[2-(2-hydroxyethoxy)ethyl]homopiperazin-1-yl]diazen-1-ium-1,2-diolate + 2,4-Dinitrofluorobenzene (70-34-8,65727-75-5) → O2-(2,4-dinitrophenyl)-1-{[4-(2-(2-hydroxyethoxy))ethyl]piperazin-1-yl}diazen-1-ium-1,2-diolate (1362738-98-4)

Guidance literature:

With sodium hydrogencarbonate; In tetrahydrofuran; water; tert-butyl alcohol; at 20 ℃;

DOI:10.1002/pola.26059

Reference yield:

1-[2-(2-hydroxyethoxy)ethyl]piperazine (13349-82-1) → O2-(2,4-dinitrophenyl)-1-{[4-(2-(2-hydroxyethoxy))ethyl]piperazin-1-yl}diazen-1-ium-1,2-diolate (1362738-98-4)

Guidance literature:

Multi-step reaction with 2 steps

1.1: sodium methylate / tetrahydrofuran; methanol; diethyl ether / 20 °C

1.2: 24 h / 20 °C / 3102.97 Torr

2.1: sodium hydrogencarbonate / tetrahydrofuran; water; tert-butyl alcohol / 20 °C

With sodium methylate; sodium hydrogencarbonate; In tetrahydrofuran; methanol; diethyl ether; water; tert-butyl alcohol;

DOI:10.1002/pola.26059

upstream raw materials:

1-[2-(2-hydroxyethoxy)ethyl]piperazine

2,4-Dinitrofluorobenzene

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