2-benzenesulfonyl-pentanedioic acid bis-(methoxy-methyl-amide)

Base Information

• Chemical Name: 2-benzenesulfonyl-pentanedioic acid bis-(methoxy-methyl-amide)
• CAS No.: 276238-63-2
• Molecular Formula: C₁₅H₂₂N₂O₆S
• Molecular Weight: 358.415
• Mol file: 276238-63-2.mol

Synonyms:2-benzenesulfonyl-pentanedioic acid bis-(methoxy-methyl-amide)

Chemical Property of 2-benzenesulfonyl-pentanedioic acid bis-(methoxy-methyl-amide)

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-benzenesulfonyl-pentanedioic acid bis-(methoxy-methyl-amide)

There total 2 articles about 2-benzenesulfonyl-pentanedioic acid bis-(methoxy-methyl-amide) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

N-methyl-N-methoxy-3-bromopropionamide (128562-58-3) + N-methoxy-N-methyl-2-phenylsulfonylacetamide (258874-02-1) → 2-benzenesulfonyl-pentanedioic acid bis-(methoxy-methyl-amide) (276238-63-2)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 24h;

DOI:10.1055/s-2000-6337

Reference yield:

N-methoxy-N-methyl-2-(phenylthio)acetamide (191731-37-0) → 2-benzenesulfonyl-pentanedioic acid bis-(methoxy-methyl-amide) (276238-63-2)

Guidance literature:

Multi-step reaction with 2 steps

1: H₂O₂; Ac₂O / H₂O; acetic acid / 8 h / 20 °C

2: 67 percent / K₂CO₃ / dimethylformamide / 24 h / 20 °C

With dihydrogen peroxide; acetic anhydride; potassium carbonate; In water; acetic acid; N,N-dimethyl-formamide; 1: Oxidation / 2: Alkylation;

DOI:10.1055/s-2000-6337

upstream raw materials:

N-methyl-N-methoxy-3-bromopropionamide

N-methoxy-N-methyl-2-phenylsulfonylacetamide

N-methoxy-N-methyl-2-(phenylthio)acetamide