2-hydroxy-2-methyl-2-(1,3,4,5,6,7-hexahydro-1,3-diazepin-2-ylium)-1-(p-chlorophenylimino)thiolate

Base Information

• Chemical Name: 2-hydroxy-2-methyl-2-(1,3,4,5,6,7-hexahydro-1,3-diazepin-2-ylium)-1-(p-chlorophenylimino)thiolate
• CAS No.: 501683-38-1
• Molecular Formula: C₁₄H₁₈ClN₃OS
• Molecular Weight: 311.835

Synonyms:2-hydroxy-2-methyl-2-(1,3,4,5,6,7-hexahydro-1,3-diazepin-2-ylium)-1-(p-chlorophenylimino)thiolate

Chemical Property of 2-hydroxy-2-methyl-2-(1,3,4,5,6,7-hexahydro-1,3-diazepin-2-ylium)-1-(p-chlorophenylimino)thiolate

Chemical Property:

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Technology Process of 2-hydroxy-2-methyl-2-(1,3,4,5,6,7-hexahydro-1,3-diazepin-2-ylium)-1-(p-chlorophenylimino)thiolate

There total 1 articles about 2-hydroxy-2-methyl-2-(1,3,4,5,6,7-hexahydro-1,3-diazepin-2-ylium)-1-(p-chlorophenylimino)thiolate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1,4-diaminobutane (110-60-1) + N-(4-chloro-phenyl)-2-methoxy-3-oxo-2-phenylamino-thiobutyramide → 2-hydroxy-2-methyl-2-(1,3,4,5,6,7-hexahydro-1,3-diazepin-2-ylium)-1-(p-chlorophenylimino)thiolate (501683-38-1)

Guidance literature:

In toluene; at 75 ℃; for 0.0833333h;

DOI:10.1055/s-2002-34866

Reference yield: 68.0%

C14H18ClN3OS (501683-38-1) + dimethyl acetylenedicarboxylate (762-42-5) → 12-(4'-chlorophenyl)-13-oxa-2-oxo-10-methyl-11-thioxo-3,8,12-triazatricyclo[8.2.1.0(3,9)]tridec-8-en-1-ylacetic acid methyl ester (1233927-74-6)

Guidance literature:

In methanol; for 0.666667h; Reflux;

DOI:10.1055/s-0029-1218710

Reference yield: 66.0%

thiophosgene (463-71-8) + 2-hydroxy-2-methyl-2-(1,3,4,5,6,7-hexahydro-1,3-diazepin-2-ylium)-1-(p-chlorophenylimino)thiolate (501683-38-1) → 2,3,4,5,7,9-hexahydro-9-methyl-9-(N-p-chlorophenylthio-carbamoyl)-[1,3]oxazolo[3,4-a][1,3]diazepin-7-thione

Guidance literature:

With sodium hydrogencarbonate; In chloroform; at 0 ℃; for 0.666667h;

DOI:10.1055/s-2002-34866

upstream raw materials:

1,4-diaminobutane

Downstream raw materials:

N,N'-bis(4-chlorophenyl)urea

bis(diphenyl)urea

1,3-Dicyclohexylurea

1,3-dinaphthalen-1-ylurea

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