(2-{2-[3,3,3-tris-(4-chloro-phenyl)-propionylamino]-acetylamino}-acetylamino)-acetic acid

Base Information

Chemical Name:(2-{2-[3,3,3-tris-(4-chloro-phenyl)-propionylamino]-acetylamino}-acetylamino)-acetic acid
CAS No.:556810-26-5
Molecular Formula:C₂₇H₂₄Cl₃N₃O₅
Molecular Weight:576.864
Hs Code.:

Synonyms:(2-{2-[3,3,3-tris-(4-chloro-phenyl)-propionylamino]-acetylamino}-acetylamino)-acetic acid

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Chemical Property of (2-{2-[3,3,3-tris-(4-chloro-phenyl)-propionylamino]-acetylamino}-acetylamino)-acetic acid

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Technology Process of (2-{2-[3,3,3-tris-(4-chloro-phenyl)-propionylamino]-acetylamino}-acetylamino)-acetic acid

There total 2 articles about (2-{2-[3,3,3-tris-(4-chloro-phenyl)-propionylamino]-acetylamino}-acetylamino)-acetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 556-33-2
glycine-glycine-glycine

: 2172-49-8
3,3,3-tris(4-chlorophenyl)propanoyl chloride

: 556810-26-5
(2-{2-[3,3,3-tris-(4-chloro-phenyl)-propionylamino]-acetylamino}-acetylamino)-acetic acid

Guidance literature:: With sodium hydroxide; In tetrahydrofuran; water; for 1h;
DOI:10.1021/ol0344927

Reference yield:

: 2168-06-1
3,3,3-Tris(4-chlorophenyl)-propionic acid

: 556810-26-5
(2-{2-[3,3,3-tris-(4-chloro-phenyl)-propionylamino]-acetylamino}-acetylamino)-acetic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / oxalyl chloride / toluene / 24 h / 20 °C

2: 63 percent / sodium hydroxide / H₂O; tetrahydrofuran / 1 h

With sodium hydroxide; oxalyl dichloride; In tetrahydrofuran; water; toluene;
DOI:10.1021/ol0344927

Reference yield: 33.3%

: 112-43-6
10-Undecen-1-ol

: 556810-26-5
(2-{2-[3,3,3-tris-(4-chloro-phenyl)-propionylamino]-acetylamino}-acetylamino)-acetic acid

: 556810-29-8
(2-{2-[3,3,3-tris-(4-chloro-phenyl)-propionylamino]-acetylamino}-acetylamino)-acetic acid undec-10-enyl ester

Guidance literature:: With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In N,N-dimethyl-formamide; at 0 - 20 ℃; for 24h;
DOI:10.1021/ol0344927