(2-{2-[3,3,3-tris-(4-chloro-phenyl)-propionylamino]-acetylamino}-acetylamino)-acetic acid undec-10-enyl ester

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Chemical Name:(2-{2-[3,3,3-tris-(4-chloro-phenyl)-propionylamino]-acetylamino}-acetylamino)-acetic acid undec-10-enyl ester
CAS No.:556810-29-8
Molecular Formula:C₃₈H₄₄Cl₃N₃O₅
Molecular Weight:729.143
Hs Code.:

Synonyms:(2-{2-[3,3,3-tris-(4-chloro-phenyl)-propionylamino]-acetylamino}-acetylamino)-acetic acid undec-10-enyl ester

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Chemical Property of (2-{2-[3,3,3-tris-(4-chloro-phenyl)-propionylamino]-acetylamino}-acetylamino)-acetic acid undec-10-enyl ester

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Technology Process of (2-{2-[3,3,3-tris-(4-chloro-phenyl)-propionylamino]-acetylamino}-acetylamino)-acetic acid undec-10-enyl ester

There total 4 articles about (2-{2-[3,3,3-tris-(4-chloro-phenyl)-propionylamino]-acetylamino}-acetylamino)-acetic acid undec-10-enyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 33.3%

: 112-43-6
10-Undecen-1-ol

: 556810-26-5
(2-{2-[3,3,3-tris-(4-chloro-phenyl)-propionylamino]-acetylamino}-acetylamino)-acetic acid

: 556810-29-8
(2-{2-[3,3,3-tris-(4-chloro-phenyl)-propionylamino]-acetylamino}-acetylamino)-acetic acid undec-10-enyl ester

Guidance literature:: With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In N,N-dimethyl-formamide; at 0 - 20 ℃; for 24h;
DOI:10.1021/ol0344927

Reference yield:

: 556-33-2
glycine-glycine-glycine

: 556810-29-8
(2-{2-[3,3,3-tris-(4-chloro-phenyl)-propionylamino]-acetylamino}-acetylamino)-acetic acid undec-10-enyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 63 percent / sodium hydroxide / H₂O; tetrahydrofuran / 1 h

2: 33.3 percent / 4-(dimethylamino)pyridine; EDCI / dimethylformamide / 24 h / 0 - 20 °C

With dmap; sodium hydroxide; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In tetrahydrofuran; water; N,N-dimethyl-formamide;
DOI:10.1021/ol0344927

Reference yield:

: 2168-06-1
3,3,3-Tris(4-chlorophenyl)-propionic acid

: 556810-29-8
(2-{2-[3,3,3-tris-(4-chloro-phenyl)-propionylamino]-acetylamino}-acetylamino)-acetic acid undec-10-enyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 90 percent / oxalyl chloride / toluene / 24 h / 20 °C

2: 63 percent / sodium hydroxide / H₂O; tetrahydrofuran / 1 h

3: 33.3 percent / 4-(dimethylamino)pyridine; EDCI / dimethylformamide / 24 h / 0 - 20 °C

With dmap; sodium hydroxide; oxalyl dichloride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In tetrahydrofuran; water; N,N-dimethyl-formamide; toluene;
DOI:10.1021/ol0344927