Methyl 2-(benzyloxy)-5-iodobenzoate

Base Information

Chemical Name:Methyl 2-(benzyloxy)-5-iodobenzoate
CAS No.:146335-26-4
Molecular Formula:C₁₅H₁₃IO₃
Molecular Weight:368.171
Hs Code.:
DSSTox Substance ID:DTXSID60446248

Synonyms:methyl 2-(benzyloxy)-5-iodobenzoate;146335-26-4;Methyl2-(benzyloxy)-5-iodobenzoate;SCHEMBL6680832;DTXSID60446248;methyl 2-benzyloxy-5-iodobenzoate;YVAHIUJFVCAHBL-UHFFFAOYSA-N;methyl 2-benzyloxy-5-iodo-benzoate;methyl 5-iodo-2-phenylmethoxybenzoate;AKOS015852005;AM80973;FT-0653938;A808488

Suppliers and Price of Methyl 2-(benzyloxy)-5-iodobenzoate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
METHYL 2-(BENZYLOXY)-5-IODOBENZOATE 95.00%
5G
$ 909.56

Alichem
Methyl2-(benzyloxy)-5-iodobenzoate
1g
$ 400.00

Total 6 raw suppliers

Chemical Property of Methyl 2-(benzyloxy)-5-iodobenzoate

Chemical Property:

XLogP3:3.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:5
Exact Mass:367.99094
Heavy Atom Count:19
Complexity:289

Purity/Quality:

97% ^*data from raw suppliers

METHYL 2-(BENZYLOXY)-5-IODOBENZOATE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC(=O)C1=C(C=CC(=C1)I)OCC2=CC=CC=C2

Technology Process of Methyl 2-(benzyloxy)-5-iodobenzoate

There total 3 articles about Methyl 2-(benzyloxy)-5-iodobenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 186581-53-3,908094-01-9,334-88-3
diazomethane

: 146335-32-2
2-benzyloxy-5-iodobenzoic acid

: 146335-26-4
methyl 2-benzyloxy-5-iodobenzoate

Guidance literature:: In methanol; diethyl ether;
DOI:10.1055/s-1992-26351

Reference yield:

: 4068-75-1
methyl 5-iodosalicylate

: 100-39-0
benzyl bromide

: 146335-26-4
methyl 2-benzyloxy-5-iodobenzoate

Guidance literature:: With potassium carbonate; In DMF (N,N-dimethyl-formamide); at 20 ℃; for 45h;

Reference yield:

: 134038-89-4
2-benzyloxy-5-iodobenzaldehyde

: 146335-26-4
methyl 2-benzyloxy-5-iodobenzoate

Guidance literature:: Multi-step reaction with 2 steps

1: 92 percent / NaClO₄, amidosulfonic acid / H₂O; dioxane / 0.5 h / Ambient temperature

2: 98 percent / methanol; diethyl ether

With aminosulfonic acid; sodium perchlorate; In 1,4-dioxane; methanol; diethyl ether; water;
DOI:10.1055/s-1992-26351