Technology Process of C17H24BrN3O2S
There total 7 articles about C17H24BrN3O2S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: sodium azide / N,N-dimethyl-formamide / 16 h / 70 °C
2: hydrogen; palladium on activated charcoal / methanol / 16 h / 20 °C
3: dichloromethane / 16 h / 0 - 20 °C
With
sodium azide; palladium on activated charcoal; hydrogen;
In
methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1080/10426507.2012.736897
- Guidance literature:
-
Multi-step reaction with 6 steps
1: sodium hydrogencarbonate / water; tetrahydrofuran / 16 h / 0 - 20 °C
2: dimethylsulfide borane complex / tetrahydrofuran / 4 h / 0 °C / Reflux
3: triethylamine / dichloromethane / 16 h / 0 - 20 °C
4: sodium azide / N,N-dimethyl-formamide / 16 h / 70 °C
5: hydrogen; palladium on activated charcoal / methanol / 16 h / 20 °C
6: dichloromethane / 16 h / 0 - 20 °C
With
sodium azide; dimethylsulfide borane complex; palladium on activated charcoal; hydrogen; sodium hydrogencarbonate; triethylamine;
In
tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1080/10426507.2012.736897
- Guidance literature:
-
Multi-step reaction with 2 steps
1: hydrogen; palladium on activated charcoal / methanol / 16 h / 20 °C
2: dichloromethane / 16 h / 0 - 20 °C
With
palladium on activated charcoal; hydrogen;
In
methanol; dichloromethane;
DOI:10.1080/10426507.2012.736897