(3R,4R)-4,5-bis((tert-butyldimethylsilyl)oxy)-3-isopropylpentyl benzoate

Base Information

Chemical Name:(3R,4R)-4,5-bis((tert-butyldimethylsilyl)oxy)-3-isopropylpentyl benzoate
CAS No.:1375478-67-3
Molecular Formula:C₂₇H₅₀O₄Si₂
Molecular Weight:494.863
Hs Code.:

Synonyms:(3R,4R)-4,5-bis((tert-butyldimethylsilyl)oxy)-3-isopropylpentyl benzoate

Suppliers and Price of (3R,4R)-4,5-bis((tert-butyldimethylsilyl)oxy)-3-isopropylpentyl benzoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (3R,4R)-4,5-bis((tert-butyldimethylsilyl)oxy)-3-isopropylpentyl benzoate

Chemical Property:

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Technology Process of (3R,4R)-4,5-bis((tert-butyldimethylsilyl)oxy)-3-isopropylpentyl benzoate

There total 6 articles about (3R,4R)-4,5-bis((tert-butyldimethylsilyl)oxy)-3-isopropylpentyl benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1375478-66-2
C₁₅H₂₂O₄

: 18162-48-6
tert-butyldimethylsilyl chloride

: 1375478-67-3
(3R,4R)-4,5-bis((tert-butyldimethylsilyl)oxy)-3-isopropylpentyl benzoate

Guidance literature:: With 1H-imidazole; dmap; In dichloromethane; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1002/anie.201108564

Reference yield:

: 1375478-63-9
ethyl (R)-3-((R)-2,2-dimethyl-1,3-dioxolan-4-yl)-4-methylpentanoate

: 1375478-67-3
(3R,4R)-4,5-bis((tert-butyldimethylsilyl)oxy)-3-isopropylpentyl benzoate

Guidance literature:: Multi-step reaction with 4 steps

1: lithium aluminium tetrahydride / tetrahydrofuran; diethyl ether / 2 h / 0 °C / Inert atmosphere

2: dmap; triethylamine / dichloromethane / 0 - 20 °C / Inert atmosphere

3: water; acetic acid / 2 h / 20 - 50 °C

4: 1H-imidazole; dmap / dichloromethane / 0 - 20 °C / Inert atmosphere

With 1H-imidazole; dmap; lithium aluminium tetrahydride; water; acetic acid; triethylamine; In tetrahydrofuran; diethyl ether; dichloromethane;
DOI:10.1002/anie.201108564

Reference yield:

: 1375478-65-1
C₁₈H₂₆O₄

: 1375478-67-3
(3R,4R)-4,5-bis((tert-butyldimethylsilyl)oxy)-3-isopropylpentyl benzoate

Guidance literature:: Multi-step reaction with 2 steps

1: water; acetic acid / 2 h / 20 - 50 °C

2: 1H-imidazole; dmap / dichloromethane / 0 - 20 °C / Inert atmosphere

With 1H-imidazole; dmap; water; acetic acid; In dichloromethane;
DOI:10.1002/anie.201108564