N-[1-(6-tert-butyl-1,1-dimethyl-2,3-dihydroinden-4-yl)ethylidene]hydroxylamine

Base Information

Chemical Name:N-[1-(6-tert-butyl-1,1-dimethyl-2,3-dihydroinden-4-yl)ethylidene]hydroxylamine
CAS No.:175136-27-3
Molecular Formula:C17H25 N O
Molecular Weight:259.38600
Hs Code.:2928000090
DSSTox Substance ID:DTXSID20352391
Mol file:175136-27-3.mol

Synonyms:N-[1-(6-tert-butyl-1,1-dimethyl-2,3-dihydroinden-4-yl)ethylidene]hydroxylamine;175136-27-3;Maybridge1_001942;DTXSID20352391;AKOS030661063;FT-0607167

Suppliers and Price of N-[1-(6-tert-butyl-1,1-dimethyl-2,3-dihydroinden-4-yl)ethylidene]hydroxylamine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
1-[6-(TERT-BUTYL)-1,1-DIMETHYL-2,3-DIHYDRO-1H-INDEN-4-YL]ETHAN-1-ONE OXIME 95.00%
250G
$ 4827.96

AHH
1-[6-(tert-Butyl)-1,1-dimethyl-2,3-dihydro-1H-inden-4-yl]ethan-1oneoxime 97%
250g
$ 480.00

Total 2 raw suppliers

Chemical Property of N-[1-(6-tert-butyl-1,1-dimethyl-2,3-dihydroinden-4-yl)ethylidene]hydroxylamine

Chemical Property:

Vapor Pressure:1.07E-05mmHg at 25°C
Melting Point:208oC
Boiling Point:356.3oC at 760 mmHg
Flash Point:223.3oC
PSA：32.59000
Density:1.01g/cm3
LogP:4.40610
XLogP3:5.2
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:259.193614421
Heavy Atom Count:19
Complexity:364

Purity/Quality:

98%min ^*data from raw suppliers

1-[6-(TERT-BUTYL)-1,1-DIMETHYL-2,3-DIHYDRO-1H-INDEN-4-YL]ETHAN-1-ONE OXIME 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(=NO)C1=C2CCC(C2=CC(=C1)C(C)(C)C)(C)C

Technology Process of N-[1-(6-tert-butyl-1,1-dimethyl-2,3-dihydroinden-4-yl)ethylidene]hydroxylamine

There total 4 articles about N-[1-(6-tert-butyl-1,1-dimethyl-2,3-dihydroinden-4-yl)ethylidene]hydroxylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 13171-00-1
Celestolide

: 175136-27-3
1-(6-tert-butyl-1,1-dimethyl-indan-4-yl)-ethanone oxime

Guidance literature:: With pyridine; hydroxylamine hydrochloride; In ethanol;
DOI:10.1016/j.bmcl.2005.12.003

Reference yield:

: 253185-03-4,253185-04-5
tert-butylbenzene

: 175136-27-3
1-(6-tert-butyl-1,1-dimethyl-indan-4-yl)-ethanone oxime

Guidance literature:: Multi-step reaction with 3 steps

1: 50 percent / AlCl₃ / nitromethane

2: 62 percent / AlCl₃ / CH₂Cl₂

3: NH₂OH*HCl; pyridine / ethanol

With pyridine; aluminium trichloride; hydroxylamine hydrochloride; In nitromethane; ethanol; dichloromethane; 2: Friedel-Crafts reaction;
DOI:10.1016/j.bmcl.2005.12.003

Reference yield:

: 3605-31-0
6-tert-butyl-1,1-dimethylindane

: 175136-27-3
1-(6-tert-butyl-1,1-dimethyl-indan-4-yl)-ethanone oxime

Guidance literature:: Multi-step reaction with 2 steps

1: 62 percent / AlCl₃ / CH₂Cl₂

2: NH₂OH*HCl; pyridine / ethanol

With pyridine; aluminium trichloride; hydroxylamine hydrochloride; In ethanol; dichloromethane; 1: Friedel-Crafts reaction;
DOI:10.1016/j.bmcl.2005.12.003