[2-chloro-4-(4-chloro-benzoyl)-6-fluoro-phenoxy]-acetic acid ethyl ester

Base Information

• Chemical Name: [2-chloro-4-(4-chloro-benzoyl)-6-fluoro-phenoxy]-acetic acid ethyl ester
• CAS No.: 1443037-98-6
• Molecular Formula: C₁₇H₁₃Cl₂FO₄
• Molecular Weight: 371.192

Synonyms:[2-chloro-4-(4-chloro-benzoyl)-6-fluoro-phenoxy]-acetic acid ethyl ester

Chemical Property of [2-chloro-4-(4-chloro-benzoyl)-6-fluoro-phenoxy]-acetic acid ethyl ester

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Technology Process of [2-chloro-4-(4-chloro-benzoyl)-6-fluoro-phenoxy]-acetic acid ethyl ester

There total 6 articles about [2-chloro-4-(4-chloro-benzoyl)-6-fluoro-phenoxy]-acetic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

(3-chloro-5-fluoro-4-hydroxy-phenyl)-(4-chloro-phenyl)-methanone (1443037-93-1) + ethyl bromoacetate (105-36-2) → [2-chloro-4-(4-chloro-benzoyl)-6-fluoro-phenoxy]-acetic acid ethyl ester (1443037-98-6)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; at 60 ℃; for 3h;

DOI:10.1016/j.ejmech.2013.02.040

Reference yield: 92.0%

(3-chloro-5-fluoro-4-hydroxy-phenyl)-(4-chloro-phenyl)-methanone (1443037-93-1) → [2-chloro-4-(4-chloro-benzoyl)-6-fluoro-phenoxy]-acetic acid ethyl ester (1443037-98-6)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; at 60 ℃; for 3h;

DOI:10.1016/j.bioorg.2016.02.001

Reference yield: 91.0%

(3-chloro-5-fluoro-4-hydroxy-phenyl)-(4-chloro-phenyl)-methanone (1443037-93-1) + chloroacetic acid ethyl ester (105-39-5) → [2-chloro-4-(4-chloro-benzoyl)-6-fluoro-phenoxy]-acetic acid ethyl ester (1443037-98-6)

Guidance literature:

With potassium carbonate; In acetone; at 60 ℃;

DOI:10.1007/s00044-019-02357-x

upstream raw materials:

4-chloro-benzoic acid 2-chloro-6-fluoro-phenyl ester

(3-chloro-5-fluoro-4-hydroxy-phenyl)-(4-chloro-phenyl)-methanone

ethyl bromoacetate

4-chloro-benzoyl chloride

Downstream raw materials:

2-(2-chloro-4-(4-chlorobenzoyl)-6-fluorophenoxy)acetohydrazide

C₃₀H₁₈Cl₃F₃N₂O₆

C₃₀H₁₈Cl₄F₂N₂O₆

C₃₁H₂₁Cl₃F₂N₂O₆

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