3-(2,4-Dimethoxyphenyl)-3-phenylallylalkohol

Base Information

• Chemical Name: 3-(2,4-Dimethoxyphenyl)-3-phenylallylalkohol
• CAS No.: 10386-54-6
• Molecular Formula: C₁₇H₁₈O₃
• Molecular Weight: 270.328
• Mol file: 10386-54-6.mol

Synonyms:3-(2,4-Dimethoxyphenyl)-3-phenylallylalkohol

Chemical Property of 3-(2,4-Dimethoxyphenyl)-3-phenylallylalkohol

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 3-(2,4-Dimethoxyphenyl)-3-phenylallylalkohol

There total 4 articles about 3-(2,4-Dimethoxyphenyl)-3-phenylallylalkohol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

3-(2-hydroxy-4-methoxyphenyl)-3-phenyl allyl alcohol (10386-53-5) + methyl iodide (74-88-4) → 3-(2,4-Dimethoxyphenyl)-3-phenylallylalkohol (10386-54-6)

Guidance literature:

With potassium carbonate; In acetone; Heating;

DOI:10.1021/ol990961m

Reference yield:

7-methoxy-4-phenyl-2H-chromen-2-one (2555-31-9) → 3-(2,4-Dimethoxyphenyl)-3-phenylallylalkohol (10386-54-6)

Guidance literature:

Multi-step reaction with 2 steps

1: 97 percent / LiAlH₄ / tetrahydrofuran; diethyl ether / 0 °C

2: 100 percent / potassium carbonate / acetone / Heating

With lithium aluminium tetrahydride; potassium carbonate; In tetrahydrofuran; diethyl ether; acetone;

DOI:10.1021/ol990961m

Reference yield:

→ 3-(2,4-Dimethoxyphenyl)-3-phenylallylalkohol (10386-54-6)

Guidance literature:

Allylalkohol VI, CH3I, K2CO3, wfr. Acn.;

upstream raw materials:

3-(2-hydroxy-4-methoxyphenyl)-3-phenyl allyl alcohol

methyl iodide

7-methoxy-4-phenyl-2H-chromen-2-one

Downstream raw materials:

(R)-3-(2,4-dimethoxyphenyl)-3-phenylpropan-1-ol

(S)-3-(2,4-dimethoxyphenyl)-3-phenylpropan-1-ol

(S)-1-phenylseleno-3-(2',4'-dimethoxyphenyl)-3-phenylpropane

(R)-3-(2',4'-dimethoxyphenyl)-3-phenyl-1-propene