1-benzyl-3-(2-((tert-butoxycarbonyl)amino)ethyl)-1H-imidazol-3-ium bromide

Base Information

Chemical Name:1-benzyl-3-(2-((tert-butoxycarbonyl)amino)ethyl)-1H-imidazol-3-ium bromide
CAS No.:1332748-29-4
Molecular Formula:Br*C₁₇H₂₄N₃O₂
Molecular Weight:382.3
Hs Code.:

Synonyms:1-benzyl-3-(2-((tert-butoxycarbonyl)amino)ethyl)-1H-imidazol-3-ium bromide

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Chemical Property of 1-benzyl-3-(2-((tert-butoxycarbonyl)amino)ethyl)-1H-imidazol-3-ium bromide

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Technology Process of 1-benzyl-3-(2-((tert-butoxycarbonyl)amino)ethyl)-1H-imidazol-3-ium bromide

There total 4 articles about 1-benzyl-3-(2-((tert-butoxycarbonyl)amino)ethyl)-1H-imidazol-3-ium bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 558441-67-1
(2-imidazol-1-yl-ethyl)-carbamic acid tert-butyl ester

: 100-39-0
benzyl bromide

: 1332748-29-4
1-benzyl-3-(2-((tert-butoxycarbonyl)amino)ethyl)-1H-imidazol-3-ium bromide

Guidance literature:: In dichloromethane; at 20 ℃; for 12h; Inert atmosphere;
DOI:10.1021/om200631w

Reference yield:

: 4238-71-5
1-benzylimidazole

: 39684-80-5
2-(tert-butoxycarbonylamino)ethyl bromide

: 1332748-29-4
1-benzyl-3-(2-((tert-butoxycarbonyl)amino)ethyl)-1H-imidazol-3-ium bromide

Guidance literature:: In tetrahydrofuran; at 75 ℃; for 12h;

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 1332748-29-4
1-benzyl-3-(2-((tert-butoxycarbonyl)amino)ethyl)-1H-imidazol-3-ium bromide

Guidance literature:: Multi-step reaction with 2 steps

1.1: trimethylamine / tetrahydrofuran / 0.5 h

1.2: Cooling with ice

2.1: tetrahydrofuran / 12 h / 75 °C

With trimethylamine; In tetrahydrofuran;