2',5-dihydroxy-3',5',6,7-tetramethoxyflavone

Base Information

Chemical Name:2',5-dihydroxy-3',5',6,7-tetramethoxyflavone
CAS No.:93092-13-8
Molecular Formula:C₁₉H₁₈O₈
Molecular Weight:374.347
Hs Code.:

Synonyms:2',5-dihydroxy-3',5',6,7-tetramethoxyflavone

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Chemical Property of 2',5-dihydroxy-3',5',6,7-tetramethoxyflavone

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Technology Process of 2',5-dihydroxy-3',5',6,7-tetramethoxyflavone

There total 7 articles about 2',5-dihydroxy-3',5',6,7-tetramethoxyflavone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 93092-12-7
2'-hydroxy-3',5,5',6,7-pentamethoxyflavone

: 93092-13-8
2',5-dihydroxy-3',5',6,7-tetramethoxyflavone

Guidance literature:: With boron trichloride; In dichloromethane;

Reference yield:

: 36873-96-8
2,3,5-trimethoxybenzoic acid

: 93092-13-8
2',5-dihydroxy-3',5',6,7-tetramethoxyflavone

Guidance literature:: Multi-step reaction with 7 steps

1: 75 percent / BCl₃ / CH₂Cl₂ / -70 °C

2: K₂CO₃ / dimethylformamide

3: 77 percent / CF₃COOH / benzene / 3 h / Ambient temperature

4: 85 percent / KOH / pyridine / 0.33 h / 100 °C

5: H₂SO₄ / acetic acid / 1 h / Ambient temperature

6: H₂ / Pd-C / ethyl acetate

7: 69 percent / BCl₃ / CH₂Cl₂

With potassium hydroxide; sulfuric acid; hydrogen; boron trichloride; potassium carbonate; trifluoroacetic acid; palladium on activated charcoal; In pyridine; dichloromethane; acetic acid; ethyl acetate; N,N-dimethyl-formamide; benzene;

Reference yield:

: 61637-60-3
3,5-dimethoxysalicylic acid

: 93092-13-8
2',5-dihydroxy-3',5',6,7-tetramethoxyflavone

Guidance literature:: Multi-step reaction with 6 steps

1: K₂CO₃ / dimethylformamide

2: 77 percent / CF₃COOH / benzene / 3 h / Ambient temperature

3: 85 percent / KOH / pyridine / 0.33 h / 100 °C

4: H₂SO₄ / acetic acid / 1 h / Ambient temperature

5: H₂ / Pd-C / ethyl acetate

6: 69 percent / BCl₃ / CH₂Cl₂

With potassium hydroxide; sulfuric acid; hydrogen; boron trichloride; potassium carbonate; trifluoroacetic acid; palladium on activated charcoal; In pyridine; dichloromethane; acetic acid; ethyl acetate; N,N-dimethyl-formamide; benzene;