N¹-(5-isothiocyanato-2-methoxyphenyl)-N¹, N², N²-trimethylethane-1,2-diamine

Base Information

• Chemical Name: N¹-(5-isothiocyanato-2-methoxyphenyl)-N¹, N², N²-trimethylethane-1,2-diamine
• CAS No.: 943519-48-0
• Molecular Formula: C₁₃H₁₉N₃OS
• Molecular Weight: 265.379

Synonyms:N¹-(5-isothiocyanato-2-methoxyphenyl)-N¹, N², N²-trimethylethane-1,2-diamine

Chemical Property of N¹-(5-isothiocyanato-2-methoxyphenyl)-N¹, N², N²-trimethylethane-1,2-diamine

Chemical Property:

Purity/Quality:

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Technology Process of N¹-(5-isothiocyanato-2-methoxyphenyl)-N¹, N², N²-trimethylethane-1,2-diamine

There total 6 articles about N¹-(5-isothiocyanato-2-methoxyphenyl)-N¹, N², N²-trimethylethane-1,2-diamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 31.0%

N1-(2-methoxy-5-nitrophenyl)-N1, N2, N2-trimethylethane-1,2-diamine (170230-34-9) + 1,1'-Thiocarbonyldiimidazole (6160-65-2) → N1-(5-isothiocyanato-2-methoxyphenyl)-N1, N2, N2-trimethylethane-1,2-diamine (943519-48-0)

Guidance literature:

N¹-(2-methoxy-5-nitrophenyl)-N¹, N², N²-trimethylethane-1,2-diamine; With hydrogen; palladium 10% on activated carbon; In ethanol; for 1.5h; under 760.051 Torr;

1,1'-Thiocarbonyldiimidazole; In dichloromethane; at 20 ℃; for 1h;

Reference yield:

N1-(2-methoxy-5-aminophenyl)-N1,N2,N2-trimethylethane-1,2-diamine (170230-35-0) + 1,1'-Thiocarbonyldiimidazole (6160-65-2) → N1-(5-isothiocyanato-2-methoxyphenyl)-N1, N2, N2-trimethylethane-1,2-diamine (943519-48-0)

Guidance literature:

In dichloromethane; at 20 ℃; for 1h;

Reference yield:

N1-(2-methoxy-5-aminophenyl)-N1,N2,N2-trimethylethane-1,2-diamine (170230-35-0) → N1-(5-isothiocyanato-2-methoxyphenyl)-N1, N2, N2-trimethylethane-1,2-diamine (943519-48-0)

Guidance literature:

With 1,1'-Thiocarbonyldiimidazole; In dichloromethane; at 20 ℃; for 1h;

upstream raw materials:

N₁-(2-methoxy-5-aminophenyl)-N₁,N₂,N₂-trimethylethane-1,2-diamine

1,1'-Thiocarbonyldiimidazole

N¹-(2-methoxy-5-nitrophenyl)-N¹, N², N²-trimethylethane-1,2-diamine

2-bromo-4-nitroanisole

Downstream raw materials:

C₂₃H₃₃N₅O₄S

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