(1R)-4-[(3R)-3-(2,2-dimethyl-1-oxopropyloxy)]-3,5,5-trimethylcyclohex-3-enol

Base Information

Chemical Name:(1R)-4-[(3R)-3-(2,2-dimethyl-1-oxopropyloxy)]-3,5,5-trimethylcyclohex-3-enol
CAS No.:649723-26-2
Molecular Formula:C₁₈H₃₂O₃
Molecular Weight:296.45
Hs Code.:

Synonyms:(1R)-4-[(3R)-3-(2,2-dimethyl-1-oxopropyloxy)]-3,5,5-trimethylcyclohex-3-enol

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Chemical Property of (1R)-4-[(3R)-3-(2,2-dimethyl-1-oxopropyloxy)]-3,5,5-trimethylcyclohex-3-enol

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Technology Process of (1R)-4-[(3R)-3-(2,2-dimethyl-1-oxopropyloxy)]-3,5,5-trimethylcyclohex-3-enol

There total 4 articles about (1R)-4-[(3R)-3-(2,2-dimethyl-1-oxopropyloxy)]-3,5,5-trimethylcyclohex-3-enol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2,2-Dimethyl-propionic acid (R)-3-((R)-4-acetoxy-2,6,6-trimethyl-cyclohex-1-enyl)-1-methyl-propyl ester

: 649723-26-2
(1R)-4-[(3R)-3-(2,2-dimethyl-1-oxopropyloxy)]-3,5,5-trimethylcyclohex-3-enol

Guidance literature:: With sodium methylate; In methanol; at 20 ℃; for 2h;
DOI:10.1248/cpb.51.878

Reference yield:

: 322474-90-8
Acetic acid (R)-4-((R)-3-hydroxy-but-1-ynyl)-3,5,5-trimethyl-cyclohex-3-enyl ester

: 649723-26-2
(1R)-4-[(3R)-3-(2,2-dimethyl-1-oxopropyloxy)]-3,5,5-trimethylcyclohex-3-enol

Guidance literature:: Multi-step reaction with 3 steps

1: 58 percent / H₂ / Pd/C / ethanol / 3 h / 20 °C

2: pyridine / 15 h / 20 °C

3: NaOMe / methanol / 2 h / 20 °C

With pyridine; hydrogen; sodium methylate; palladium on activated charcoal; In methanol; ethanol;
DOI:10.1248/cpb.51.878

Reference yield:

: 3282-30-2
pivaloyl chloride

: 649723-26-2
(1R)-4-[(3R)-3-(2,2-dimethyl-1-oxopropyloxy)]-3,5,5-trimethylcyclohex-3-enol

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / 15 h / 20 °C

2: NaOMe / methanol / 2 h / 20 °C

With pyridine; sodium methylate; In methanol;
DOI:10.1248/cpb.51.878