5-[4,5-bis-(4-dimethylamino-phenyl)-1-methyl-1H-imidazol-2-yl]-thiophene-2-carbaldehyde

Base Information

Chemical Name:5-[4,5-bis-(4-dimethylamino-phenyl)-1-methyl-1H-imidazol-2-yl]-thiophene-2-carbaldehyde
CAS No.:335356-32-6
Molecular Formula:C₂₅H₂₆N₄OS
Molecular Weight:430.574
Hs Code.:

5-[4,5-bis-(4-dimethylamino-phenyl)-1-methyl-1<i>H</i>-imidazol-2-yl]-thiophene-2-carbaldehyde

Synonyms:5-[4,5-bis-(4-dimethylamino-phenyl)-1-methyl-1H-imidazol-2-yl]-thiophene-2-carbaldehyde

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Chemical Property of 5-[4,5-bis-(4-dimethylamino-phenyl)-1-methyl-1H-imidazol-2-yl]-thiophene-2-carbaldehyde

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Technology Process of 5-[4,5-bis-(4-dimethylamino-phenyl)-1-methyl-1H-imidazol-2-yl]-thiophene-2-carbaldehyde

There total 3 articles about 5-[4,5-bis-(4-dimethylamino-phenyl)-1-methyl-1H-imidazol-2-yl]-thiophene-2-carbaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: 68-12-2,33513-42-7
N,N-dimethyl-formamide

: 335356-28-0
C₂₄H₂₆N₄S

: 335356-32-6
5-[4,5-bis-(4-dimethylamino-phenyl)-1-methyl-1H-imidazol-2-yl]-thiophene-2-carbaldehyde

Guidance literature:: C₂₄H₂₆N₄S; With n-butyllithium; In tetrahydrofuran; at -78 - 0 ℃;

N,N-dimethyl-formamide;
DOI:10.1016/S0040-4039(00)02143-2

Reference yield:

: 17078-27-2
4,4'-bis(dimethylamino)benzil

: 335356-32-6
5-[4,5-bis-(4-dimethylamino-phenyl)-1-methyl-1H-imidazol-2-yl]-thiophene-2-carbaldehyde

Guidance literature:: Multi-step reaction with 3 steps

1: 70 percent / ammonium acetate / acetic acid / 120 °C

2: 78 percent / potassium carbonate / 55 °C

3: 53 percent / n-butyl lithium / tetrahydrofuran / -78 - 0 °C

With ammonium acetate; n-butyllithium; potassium carbonate; In tetrahydrofuran; acetic acid;
DOI:10.1016/S0040-4039(00)02143-2

Reference yield:

: 335356-27-9
C₂₃H₂₄N₄S

: 335356-32-6
5-[4,5-bis-(4-dimethylamino-phenyl)-1-methyl-1H-imidazol-2-yl]-thiophene-2-carbaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1: 78 percent / potassium carbonate / 55 °C

2: 53 percent / n-butyl lithium / tetrahydrofuran / -78 - 0 °C

With n-butyllithium; potassium carbonate; In tetrahydrofuran;
DOI:10.1016/S0040-4039(00)02143-2