N₁-(2-aminoethyl)-N₆-[(benzyloxy)carbonyl]-N₂-(tertbutoxycarbonyl)-L-lysinamide

Base Information

Chemical Name:N₁-(2-aminoethyl)-N₆-[(benzyloxy)carbonyl]-N₂-(tertbutoxycarbonyl)-L-lysinamide
CAS No.:229486-31-1
Molecular Formula:C₂₁H₃₄N₄O₅
Molecular Weight:422.525
Hs Code.:

N<sub>1</sub>-(2-aminoethyl)-N<sub>6</sub>-[(benzyloxy)carbonyl]-N<sub>2</sub>-(tertbutoxycarbonyl)-L-lysinamide

Synonyms:N₁-(2-aminoethyl)-N₆-[(benzyloxy)carbonyl]-N₂-(tertbutoxycarbonyl)-L-lysinamide

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Chemical Property of N₁-(2-aminoethyl)-N₆-[(benzyloxy)carbonyl]-N₂-(tertbutoxycarbonyl)-L-lysinamide

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Technology Process of N₁-(2-aminoethyl)-N₆-[(benzyloxy)carbonyl]-N₂-(tertbutoxycarbonyl)-L-lysinamide

There total 4 articles about N₁-(2-aminoethyl)-N₆-[(benzyloxy)carbonyl]-N₂-(tertbutoxycarbonyl)-L-lysinamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 73548-77-3
Boc-L-Lys(Z)-OMe

: 107-15-3,85404-18-8
ethylenediamine

: 229486-31-1
N₁-(2-aminoethyl)-N₆-[(benzyloxy)carbonyl]-N₂-(tertbutoxycarbonyl)-L-lysinamide

Guidance literature:: In methanol; at 20 ℃;

Reference yield: 30.0%

: 2389-45-9
Boc-Lys(Z)-OH

: 107-15-3,85404-18-8
ethylenediamine

: 229486-31-1
N₁-(2-aminoethyl)-N₆-[(benzyloxy)carbonyl]-N₂-(tertbutoxycarbonyl)-L-lysinamide

Guidance literature:: With benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 20 ℃;
DOI:10.1016/j.tet.2009.07.031

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 229486-31-1
N₁-(2-aminoethyl)-N₆-[(benzyloxy)carbonyl]-N₂-(tertbutoxycarbonyl)-L-lysinamide

Guidance literature:: Multi-step reaction with 2 steps

1: 99 percent / Et₃N / CH₂Cl₂; CHCl₃

2: 89 percent / methanol / 20 °C

With triethylamine; In methanol; dichloromethane; chloroform; 1: Condensation / 2: Substitution;