methyl (2E)-3-(3-{[(1S)-1-cyclohexyl-2-(cyclopentyloxy)-2-oxoethyl]carbamoyl}phenyl)acrylate

Base Information

Chemical Name:methyl (2E)-3-(3-{[(1S)-1-cyclohexyl-2-(cyclopentyloxy)-2-oxoethyl]carbamoyl}phenyl)acrylate
CAS No.:1018674-31-1
Molecular Formula:C₂₄H₃₁NO₅
Molecular Weight:413.514
Hs Code.:

Synonyms:methyl (2E)-3-(3-{[(1S)-1-cyclohexyl-2-(cyclopentyloxy)-2-oxoethyl]carbamoyl}phenyl)acrylate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl (2E)-3-(3-{[(1S)-1-cyclohexyl-2-(cyclopentyloxy)-2-oxoethyl]carbamoyl}phenyl)acrylate

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Technology Process of methyl (2E)-3-(3-{[(1S)-1-cyclohexyl-2-(cyclopentyloxy)-2-oxoethyl]carbamoyl}phenyl)acrylate

There total 5 articles about methyl (2E)-3-(3-{[(1S)-1-cyclohexyl-2-(cyclopentyloxy)-2-oxoethyl]carbamoyl}phenyl)acrylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 956928-36-2
cyclopentyl (2S)-amino(cyclohexyl)acetate hydrochloride

: 581799-33-9
3-[(1E)-3-methoxy-3-oxoprop-1-en-1-yl]benzoic acid chloride

: 1018674-31-1
methyl (2E)-3-(3-{[(1S)-1-cyclohexyl-2-(cyclopentyloxy)-2-oxoethyl]carbamoyl}phenyl)acrylate

Guidance literature:: With pyridine; In dichloromethane; at 20 ℃; for 18h;

Reference yield:

: 914604-31-2
(S)-tert-butoxycarbonylamino-cyclohexyl-acetic acid cyclopentyl ester

: 1018674-31-1
methyl (2E)-3-(3-{[(1S)-1-cyclohexyl-2-(cyclopentyloxy)-2-oxoethyl]carbamoyl}phenyl)acrylate

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogenchloride / 1,4-dioxane; dichloromethane / 24 h / 20 °C

2: pyridine / dichloromethane / 18 h / 20 °C

With pyridine; hydrogenchloride; In 1,4-dioxane; dichloromethane;

Reference yield:

: 619-21-6
m-formylphenyl benzoic acid

: 1018674-31-1
methyl (2E)-3-(3-{[(1S)-1-cyclohexyl-2-(cyclopentyloxy)-2-oxoethyl]carbamoyl}phenyl)acrylate

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium carbonate / water / 17 h / 0 - 20 °C

1.2: pH 1 / Acidic aqueous solution

2.1: thionyl chloride; N,N-dimethyl-formamide / toluene / 1 h / Heating / reflux

3.1: pyridine / dichloromethane / 18 h / 20 °C

With pyridine; thionyl chloride; potassium carbonate; N,N-dimethyl-formamide; In dichloromethane; water; toluene;