C₂₃H₃₂O₈

Base Information

• Chemical Name: C₂₃H₃₂O₈
• CAS No.: 1449477-28-4
• Molecular Formula: C₂₃H₃₂O₈
• Molecular Weight: 436.502
• Mol file: 1449477-28-4.mol

Synonyms:C₂₃H₃₂O₈

Chemical Property of C₂₃H₃₂O₈

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of C₂₃H₃₂O₈

There total 1 articles about C₂₃H₃₂O₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

methyl galloate (99-24-1) + pivaloyl chloride (3282-30-2) → C23H32O8 (1449477-28-4)

Guidance literature:

With pyridine; at 0 - 20 ℃; for 18.5h; Inert atmosphere;

DOI:10.1002/asia.201201168

Reference yield: 93.0%

C23H32O8 (1449477-28-4) → C22H32O7 (1449477-29-5)

Guidance literature:

With L-Selectride; In tetrahydrofuran; at -78 ℃; for 4h; Inert atmosphere;

DOI:10.1002/asia.201201168

Reference yield:

C23H32O8 (1449477-28-4) → C22H30O7 (1449477-30-8)

Guidance literature:

Multi-step reaction with 2 steps

1: L-Selectride / tetrahydrofuran / 4 h / -78 °C / Inert atmosphere

2: dipyridinium dichromate / dichloromethane / 2 h / 0 - 20 °C / Inert atmosphere

With dipyridinium dichromate; L-Selectride; In tetrahydrofuran; dichloromethane;

DOI:10.1002/asia.201201168

upstream raw materials:

methyl galloate

pivaloyl chloride

Downstream raw materials:

C₃₀H₄₈O₇Si

C₃₀H₄₈O₇Si

C₂₂H₃₂O₇

C₂₂H₃₀O₇

Refernces