Technology Process of C36H54O12
There total 4 articles about C36H54O12 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
tetrabutyl ammonium fluoride;
In
tetrahydrofuran; methanol;
at 12 ℃;
DOI:10.1139/V10-156
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 18-crown-6 ether; potassium carbonate; potassium iodide / N,N-dimethyl-formamide / 48 h / 100 °C / Inert atmosphere
2: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / tetrahydrofuran / 48 h / 20 °C / Inert atmosphere
3: tetrabutyl ammonium fluoride / tetrahydrofuran; methanol / 12 °C
With
bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; 18-crown-6 ether; tetrabutyl ammonium fluoride; potassium carbonate; triethylamine; potassium iodide;
In
tetrahydrofuran; methanol; N,N-dimethyl-formamide;
2: Sonogashira reaction;
DOI:10.1139/V10-156
- Guidance literature:
-
Multi-step reaction with 2 steps
1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / tetrahydrofuran / 48 h / 20 °C / Inert atmosphere
2: tetrabutyl ammonium fluoride / tetrahydrofuran; methanol / 12 °C
With
bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; tetrabutyl ammonium fluoride; triethylamine;
In
tetrahydrofuran; methanol;
1: Sonogashira reaction;
DOI:10.1139/V10-156