Benzyl 2-acetamido-3-O-benzoyl-2-deoxy-4,6-O-<1-(methoxycarbonyl)ethylidene>-α-D-glucopyranoside

Base Information

Chemical Name:Benzyl 2-acetamido-3-O-benzoyl-2-deoxy-4,6-O-<1-(methoxycarbonyl)ethylidene>-α-D-glucopyranoside
CAS No.:143836-21-9
Molecular Formula:C₂₆H₂₉NO₉
Molecular Weight:499.518
Hs Code.:

Synonyms:Benzyl 2-acetamido-3-O-benzoyl-2-deoxy-4,6-O-<1-(methoxycarbonyl)ethylidene>-α-D-glucopyranoside

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Chemical Property of Benzyl 2-acetamido-3-O-benzoyl-2-deoxy-4,6-O-<1-(methoxycarbonyl)ethylidene>-α-D-glucopyranoside

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Technology Process of Benzyl 2-acetamido-3-O-benzoyl-2-deoxy-4,6-O-<1-(methoxycarbonyl)ethylidene>-α-D-glucopyranoside

There total 5 articles about Benzyl 2-acetamido-3-O-benzoyl-2-deoxy-4,6-O-<1-(methoxycarbonyl)ethylidene>-α-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 600-22-6
pyruvic acid methyl ester

: 145259-91-2
Benzoic acid (2S,3R,4R,4aS,10aR)-3-acetylamino-2-benzyloxy-6,6,8,8-tetraisopropyl-hexahydro-1,5,7,9-tetraoxa-6,8-disila-benzocycloocten-4-yl ester

: 143836-21-9
Benzyl 2-acetamido-3-O-benzoyl-2-deoxy-4,6-O-<1-(methoxycarbonyl)ethylidene>-α-D-glucopyranoside

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; for 15h; Ambient temperature;
DOI:10.1055/s-1992-26291

Reference yield: 83.0%

: 600-22-6
pyruvic acid methyl ester

: 33423-31-3
benzyl 2-acetamido-3-O-benzoyl-2-deoxy-α-D-glucopyranoside

: 143836-21-9
Benzyl 2-acetamido-3-O-benzoyl-2-deoxy-4,6-O-<1-(methoxycarbonyl)ethylidene>-α-D-glucopyranoside

Guidance literature:: With boron trifluoride diethyl etherate; In dichloromethane; for 24h; Ambient temperature;
DOI:10.1016/S0040-4039(00)60097-7

Reference yield:

: 618-32-6
Benzoyl bromide

: 143836-21-9
Benzyl 2-acetamido-3-O-benzoyl-2-deoxy-4,6-O-<1-(methoxycarbonyl)ethylidene>-α-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 63 percent / pyridine / 60 °C

2: 98 percent / trimethylsilyl trifluoromethanesulfonate / CH₂Cl₂ / 15 h / Ambient temperature

With pyridine; trimethylsilyl trifluoromethanesulfonate; In dichloromethane;
DOI:10.1055/s-1992-26291