2-Ethoxy-1-methyl-4-phenyl-2-<(p-trifluormethyl)phenyl>-1,2-dihydro-4H-3,1-benzoxazin

Base Information

Chemical Name:2-Ethoxy-1-methyl-4-phenyl-2-<(p-trifluormethyl)phenyl>-1,2-dihydro-4H-3,1-benzoxazin
CAS No.:86839-41-0
Molecular Formula:C₂₄H₂₂F₃NO₂
Molecular Weight:413.439
Hs Code.:

Synonyms:2-Ethoxy-1-methyl-4-phenyl-2-<(p-trifluormethyl)phenyl>-1,2-dihydro-4H-3,1-benzoxazin

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Chemical Property of 2-Ethoxy-1-methyl-4-phenyl-2-<(p-trifluormethyl)phenyl>-1,2-dihydro-4H-3,1-benzoxazin

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Technology Process of 2-Ethoxy-1-methyl-4-phenyl-2-<(p-trifluormethyl)phenyl>-1,2-dihydro-4H-3,1-benzoxazin

There total 4 articles about 2-Ethoxy-1-methyl-4-phenyl-2-<(p-trifluormethyl)phenyl>-1,2-dihydro-4H-3,1-benzoxazin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 141-52-6
sodium ethanolate

: 1-Methyl-4-phenyl-2-(p-trifluormethylphenyl)-4H-3,1-benzoxazinium-fluorsulfonat

: 86839-41-0
2-Ethoxy-1-methyl-4-phenyl-2-<(p-trifluormethyl)phenyl>-1,2-dihydro-4H-3,1-benzoxazin

Guidance literature:: at 0 ℃;

Reference yield:

: 86839-12-5
2-<(p-Trifluormethyl)benzoylamino>benzophenon

: 86839-41-0
2-Ethoxy-1-methyl-4-phenyl-2-<(p-trifluormethyl)phenyl>-1,2-dihydro-4H-3,1-benzoxazin

Guidance literature:: Multi-step reaction with 4 steps

1: 97 percent / NaBH₄

2: 70 percent / PBr₃ / CH₂Cl₂

3: 90 percent / CH₂Cl₂ / 12 h / Ambient temperature

4: 84 percent / 0 °C

With sodium tetrahydroborate; phosphorus tribromide; In dichloromethane;

Reference yield:

: 86839-17-0
p-(Trifluormethyl)benzoesaeure-(α-hydroxy-α-phenyl-o-toluidid)

: 86839-41-0
2-Ethoxy-1-methyl-4-phenyl-2-<(p-trifluormethyl)phenyl>-1,2-dihydro-4H-3,1-benzoxazin

Guidance literature:: Multi-step reaction with 3 steps

1: 70 percent / PBr₃ / CH₂Cl₂

2: 90 percent / CH₂Cl₂ / 12 h / Ambient temperature

3: 84 percent / 0 °C

With phosphorus tribromide; In dichloromethane;