1-(2-bromophenyl)-5,6-dihydro-8,9-dimethoxypyrrolo[2,1-a]isoquinoline-2,3-dione

Base Information

Chemical Name:1-(2-bromophenyl)-5,6-dihydro-8,9-dimethoxypyrrolo[2,1-a]isoquinoline-2,3-dione
CAS No.:80041-84-5
Molecular Formula:C₂₀H₁₆BrNO₄
Molecular Weight:414.255
Hs Code.:

Synonyms:1-(2-bromophenyl)-5,6-dihydro-8,9-dimethoxypyrrolo[2,1-a]isoquinoline-2,3-dione

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Chemical Property of 1-(2-bromophenyl)-5,6-dihydro-8,9-dimethoxypyrrolo[2,1-a]isoquinoline-2,3-dione

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Technology Process of 1-(2-bromophenyl)-5,6-dihydro-8,9-dimethoxypyrrolo[2,1-a]isoquinoline-2,3-dione

There total 7 articles about 1-(2-bromophenyl)-5,6-dihydro-8,9-dimethoxypyrrolo[2,1-a]isoquinoline-2,3-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 79-37-8
oxalyl dichloride

: 80041-81-2
1-(2-bromobenzyl)-3,4-dihydro-6,7-dimethoxyisoquinoline

: 80041-84-5
1-(2-bromophenyl)-5,6-dihydro-8,9-dimethoxypyrrolo[2,1-a]isoquinoline-2,3-dione

Guidance literature:: With pyridine; for 2h; Ambient temperature;
DOI:10.1021/jo00342a028

Reference yield: 78.0%

: 3382-18-1
6,7-dimethoxy-3,4-dihydro-isoquinoline

: 1026775-98-3
C₁₀H₉BrO₃

: 80041-84-5
1-(2-bromophenyl)-5,6-dihydro-8,9-dimethoxypyrrolo[2,1-a]isoquinoline-2,3-dione

Guidance literature:: With sodium methylate; In N,N-dimethyl-formamide; at 150 ℃; for 0.166667h; under 5171.62 Torr; microwave irradiation;
DOI:10.1055/s-2008-1042764

Reference yield: 77.0%

: 3382-18-1
6,7-dimethoxy-3,4-dihydro-isoquinoline

: 1026775-99-4
C₁₁H₁₀BrClO₃

: 80041-84-5
1-(2-bromophenyl)-5,6-dihydro-8,9-dimethoxypyrrolo[2,1-a]isoquinoline-2,3-dione

Guidance literature:: With copper; zinc; In N,N-dimethyl-formamide; at 150 ℃; for 0.166667h; under 5171.62 Torr; microwave irradiation;
DOI:10.1055/s-2008-1042764