ethyl 2-(4-cyclopropanesulfonyl-phenyl)-3-(tetrahydropyran-4-yl)propionate

Base Information

Chemical Name:ethyl 2-(4-cyclopropanesulfonyl-phenyl)-3-(tetrahydropyran-4-yl)propionate
CAS No.:745052-97-5
Molecular Formula:C₁₉H₂₆O₅S
Molecular Weight:366.478
Hs Code.:

Synonyms:ethyl 2-(4-cyclopropanesulfonyl-phenyl)-3-(tetrahydropyran-4-yl)propionate

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Chemical Property of ethyl 2-(4-cyclopropanesulfonyl-phenyl)-3-(tetrahydropyran-4-yl)propionate

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Technology Process of ethyl 2-(4-cyclopropanesulfonyl-phenyl)-3-(tetrahydropyran-4-yl)propionate

There total 13 articles about ethyl 2-(4-cyclopropanesulfonyl-phenyl)-3-(tetrahydropyran-4-yl)propionate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

: 1058167-40-0
ethyl [4-(cyclopropylsulfonyl)phenyl]acetate

: (tetrahydro-2H-pyran-4-yl)methyl trifluoromethanesulfonate

: 745052-97-5
ethyl 2-(4-cyclopropanesulfonyl-phenyl)-3-(tetrahydropyran-4-yl)propionate

Guidance literature:: ethyl [4-(cyclopropylsulfonyl)phenyl]acetate; With lithium hexamethyldisilazane; In tetrahydrofuran; at -10 - 0 ℃; for 2.5h;

(tetrahydro-2H-pyran-4-yl)methyl trifluoromethanesulfonate; With 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone; In tetrahydrofuran; at -10 - 25 ℃; for 3h;
DOI:10.1021/op400354g

Reference yield: 57.0%

: 1058167-40-0
ethyl [4-(cyclopropylsulfonyl)phenyl]acetate

: 132291-95-3
4-(methanesulfonyloxymethyl)tetrahydropyran

: 745052-97-5
ethyl 2-(4-cyclopropanesulfonyl-phenyl)-3-(tetrahydropyran-4-yl)propionate

Guidance literature:: ethyl [4-(cyclopropylsulfonyl)phenyl]acetate; With lithium hexamethyldisilazane; In tetrahydrofuran; at -10 - 0 ℃; for 2.5h;

4-(methanesulfonyloxymethyl)tetrahydropyran; With 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone; In tetrahydrofuran; at -10 - 25 ℃; for 3h;
DOI:10.1021/op400354g

Reference yield: 33.0%

: 1058167-40-0
ethyl [4-(cyclopropylsulfonyl)phenyl]acetate

: 101691-65-0
toluene-4-sulfonic acid tetrahydropyran-4-ylmethyl ester

: 745052-97-5
ethyl 2-(4-cyclopropanesulfonyl-phenyl)-3-(tetrahydropyran-4-yl)propionate

Guidance literature:: ethyl [4-(cyclopropylsulfonyl)phenyl]acetate; With lithium hexamethyldisilazane; In tetrahydrofuran; at -10 - 0 ℃; for 2.5h;

toluene-4-sulfonic acid tetrahydropyran-4-ylmethyl ester; With 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone; In tetrahydrofuran; at -10 - 25 ℃; for 3h;
DOI:10.1021/op400354g