ethyl 2-(4-(cyclopropylsulfonyl)phenyl)-3-(tetrahydro-2H-pyran-4-yl)acrylate

Base Information

Chemical Name:ethyl 2-(4-(cyclopropylsulfonyl)phenyl)-3-(tetrahydro-2H-pyran-4-yl)acrylate
CAS No.:745052-96-4
Molecular Formula:C₁₉H₂₄O₅S
Molecular Weight:364.463
Hs Code.:

Synonyms:ethyl 2-(4-(cyclopropylsulfonyl)phenyl)-3-(tetrahydro-2H-pyran-4-yl)acrylate

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Chemical Property of ethyl 2-(4-(cyclopropylsulfonyl)phenyl)-3-(tetrahydro-2H-pyran-4-yl)acrylate

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:: SDS file from LookChem

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Technology Process of ethyl 2-(4-(cyclopropylsulfonyl)phenyl)-3-(tetrahydro-2H-pyran-4-yl)acrylate

There total 4 articles about ethyl 2-(4-(cyclopropylsulfonyl)phenyl)-3-(tetrahydro-2H-pyran-4-yl)acrylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 50675-18-8
3,4,5,6-tetrahydro-2H-pyran-4-carbaldehyde

: 876063-40-0
(4-cyclopropylsulfonylphenyl)-2-oxo-acetic acid ethyl ester

: 745052-96-4
ethyl 2-(4-(cyclopropylsulfonyl)phenyl)-3-(tetrahydro-2H-pyran-4-yl)acrylate

Guidance literature:: With titanium tetrachloride; zinc; In tetrahydrofuran;

Reference yield:

: 745052-95-3
ethyl 2-(4-(cyclopropylthio)phenyl)-3-(tetrahydro-2H-pyran-4-yl)acrylate

: 745052-96-4
ethyl 2-(4-(cyclopropylsulfonyl)phenyl)-3-(tetrahydro-2H-pyran-4-yl)acrylate

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; for 16h;

Reference yield:

: 745052-94-2
ethyl 2-(4-cyclopropylsulfanylphenyl)-2-oxoacetate

: 745052-92-0
triphenyl((tetrahydro-2H-pyran-4-yl)methyl)phosphonium iodide

: 745052-96-4
ethyl 2-(4-(cyclopropylsulfonyl)phenyl)-3-(tetrahydro-2H-pyran-4-yl)acrylate

Guidance literature:: triphenyl((tetrahydro-2H-pyran-4-yl)methyl)phosphonium iodide; With lithium hexamethyldisilazane; In tetrahydrofuran; at 0 - 20 ℃; for 3h; Large scale reaction;

ethyl 2-(4-cyclopropylsulfanylphenyl)-2-oxoacetate; In tetrahydrofuran; at 0 - 20 ℃; Large scale reaction;

With potassium peroxymonosulfate; In water; acetone; at 5 - 15 ℃; for 11.5h; Large scale reaction;
DOI:10.1021/op300053a