benzyl (1s,4s)-4-(5-bromo-2-chloropyrimidin-4-ylamino)cyclohexylcarbamate

Base Information

Chemical Name:benzyl (1s,4s)-4-(5-bromo-2-chloropyrimidin-4-ylamino)cyclohexylcarbamate
CAS No.:1192712-36-9
Molecular Formula:C₁₈H₂₀BrClN₄O₂
Molecular Weight:439.739
Hs Code.:

Synonyms:benzyl (1s,4s)-4-(5-bromo-2-chloropyrimidin-4-ylamino)cyclohexylcarbamate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of benzyl (1s,4s)-4-(5-bromo-2-chloropyrimidin-4-ylamino)cyclohexylcarbamate

Chemical Property:

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Technology Process of benzyl (1s,4s)-4-(5-bromo-2-chloropyrimidin-4-ylamino)cyclohexylcarbamate

There total 1 articles about benzyl (1s,4s)-4-(5-bromo-2-chloropyrimidin-4-ylamino)cyclohexylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 36082-50-5
2,4-dichloro-5-bromopyrimidine

: 149423-70-1,227017-99-4
(±)-cis-N1-benzyloxycarbonyl-1,4-cyclohexanediamine

: 1192712-36-9
benzyl (1s,4s)-4-(5-bromo-2-chloropyrimidin-4-ylamino)cyclohexylcarbamate

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In acetonitrile; at 20 ℃; for 20h;

Reference yield:

: 1192712-36-9
benzyl (1s,4s)-4-(5-bromo-2-chloropyrimidin-4-ylamino)cyclohexylcarbamate

: 1692-15-5
4-pyridylboronic acid

: 1192712-37-0
benzyl (1s,4s)-4-(2-chloro-5-(pyridin-4-yl)pyrimidin-4-ylamino)cyclohexylcarbamate

Guidance literature:: With sodium carbonate; bis-triphenylphosphine-palladium(II) chloride; In 1,4-dioxane; water; at 100 ℃; for 21.5h;

Reference yield:

: 1192712-36-9
benzyl (1s,4s)-4-(5-bromo-2-chloropyrimidin-4-ylamino)cyclohexylcarbamate

: 411235-57-9
cyclopropylboronic acid

: 1192712-39-2
benzyl (1s,4s)-4-(2-chloro-5-cyclopropylpyrimidin-4-ylamino)cyclohexylcarbamate

Guidance literature:: With potassium phosphate; palladium diacetate; tricyclohexylphosphine; In water; toluene; at 100 ℃; for 20h; Inert atmosphere;