tert-butyl((1-((4-methoxybenzyl)oxy)undec-10-en-2-yl)oxy)dimethylsilane

Base Information

Chemical Name:tert-butyl((1-((4-methoxybenzyl)oxy)undec-10-en-2-yl)oxy)dimethylsilane
CAS No.:1489364-96-6
Molecular Formula:C₂₅H₄₄O₃Si
Molecular Weight:420.708
Hs Code.:

Synonyms:tert-butyl((1-((4-methoxybenzyl)oxy)undec-10-en-2-yl)oxy)dimethylsilane

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Chemical Property of tert-butyl((1-((4-methoxybenzyl)oxy)undec-10-en-2-yl)oxy)dimethylsilane

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Technology Process of tert-butyl((1-((4-methoxybenzyl)oxy)undec-10-en-2-yl)oxy)dimethylsilane

There total 1 articles about tert-butyl((1-((4-methoxybenzyl)oxy)undec-10-en-2-yl)oxy)dimethylsilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 4117-09-3
7-bromo-hept-1-ene

: 1489364-88-6
(R)-tert-butyl((1-((4-methoxybenzyl)oxy)but-3-en-2-yl)oxy)dimethylsilane

: 1489364-96-6
tert-butyl((1-((4-methoxybenzyl)oxy)undec-10-en-2-yl)oxy)dimethylsilane

Guidance literature:: (R)-tert-butyl((1-((4-methoxybenzyl)oxy)but-3-en-2-yl)oxy)dimethylsilane; With 9-borabicyclo[3.3.1]nonane dimer; In tetrahydrofuran; at 20 ℃; for 10h; Glovebox;

7-bromo-hept-1-ene; With potassium phosphate monohydrate; palladium diacetate; triphenylphosphine; In tetrahydrofuran; N,N-dimethyl-formamide; at 20 ℃; for 24h; Sealed tube;
DOI:10.1021/ja409995w

Reference yield:

: 1489364-96-6
tert-butyl((1-((4-methoxybenzyl)oxy)undec-10-en-2-yl)oxy)dimethylsilane

: 1489365-14-1
N-((3R,10R)-10-((tert-butyldimethylsilyl)oxy)-11-((4-methoxybenzyl)oxy)undec-1-en-3-yl)-4-methoxyaniline

: 1489365-13-0
N-((3S,10R)-10-((tert-butyldimethylsilyl)oxy)-11-((4-methoxybenzyl)oxy)undec-1-en-3-yl)-4-methoxyaniline

Guidance literature:: Multi-step reaction with 2 steps

1: palladium diacetate; 4,5-Diazafluoren-9-one / dodecane / 65 °C / Sealed tube

2: potassium phosphate; C₄₄H₄₁IrNO₂P / toluene / 25 °C / Glovebox

With potassium phosphate; 4,5-Diazafluoren-9-one; C₄₄H₄₁IrNO₂P; palladium diacetate; In dodecane; toluene;
DOI:10.1021/ja409995w