N-((3S,10R)-10-((tert-butyldimethylsilyl)oxy)-11-((4-methoxybenzyl)oxy)undec-1-en-3-yl)-4-methoxyaniline

Base Information

Chemical Name:N-((3S,10R)-10-((tert-butyldimethylsilyl)oxy)-11-((4-methoxybenzyl)oxy)undec-1-en-3-yl)-4-methoxyaniline
CAS No.:1489365-13-0
Molecular Formula:C₃₂H₅₁NO₄Si
Molecular Weight:541.847
Hs Code.:

Synonyms:N-((3S,10R)-10-((tert-butyldimethylsilyl)oxy)-11-((4-methoxybenzyl)oxy)undec-1-en-3-yl)-4-methoxyaniline

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Chemical Property of N-((3S,10R)-10-((tert-butyldimethylsilyl)oxy)-11-((4-methoxybenzyl)oxy)undec-1-en-3-yl)-4-methoxyaniline

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Technology Process of N-((3S,10R)-10-((tert-butyldimethylsilyl)oxy)-11-((4-methoxybenzyl)oxy)undec-1-en-3-yl)-4-methoxyaniline

There total 4 articles about N-((3S,10R)-10-((tert-butyldimethylsilyl)oxy)-11-((4-methoxybenzyl)oxy)undec-1-en-3-yl)-4-methoxyaniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4117-09-3
7-bromo-hept-1-ene

: 1489365-14-1
N-((3R,10R)-10-((tert-butyldimethylsilyl)oxy)-11-((4-methoxybenzyl)oxy)undec-1-en-3-yl)-4-methoxyaniline

: 1489365-13-0
N-((3S,10R)-10-((tert-butyldimethylsilyl)oxy)-11-((4-methoxybenzyl)oxy)undec-1-en-3-yl)-4-methoxyaniline

Guidance literature:: Multi-step reaction with 3 steps

1.1: 9-borabicyclo[3.3.1]nonane dimer / tetrahydrofuran / 10 h / 20 °C / Glovebox

1.2: polytetrafluoroethylene / 24 h / 20 °C / Sealed tube

2.1: palladium diacetate; 4,5-Diazafluoren-9-one / dodecane / 65 °C / Sealed tube

3.1: potassium phosphate; C₄₄H₄₁IrNO₂P / toluene / 25 °C / Glovebox

With potassium phosphate; 9-borabicyclo[3.3.1]nonane dimer; 4,5-Diazafluoren-9-one; C₄₄H₄₁IrNO₂P; palladium diacetate; In tetrahydrofuran; dodecane; toluene;
DOI:10.1021/ja409995w

Reference yield:

: C₃₂H₄₈O₅Si

: 104-94-9
4-methoxy-aniline

: 1489365-14-1
N-((3R,10R)-10-((tert-butyldimethylsilyl)oxy)-11-((4-methoxybenzyl)oxy)undec-1-en-3-yl)-4-methoxyaniline

: 1489365-13-0
N-((3S,10R)-10-((tert-butyldimethylsilyl)oxy)-11-((4-methoxybenzyl)oxy)undec-1-en-3-yl)-4-methoxyaniline

Guidance literature:: With potassium phosphate; C₄₄H₄₁IrNO₂P; In toluene; at 25 ℃; Overall yield = 105.6 mg; Glovebox;
DOI:10.1021/ja409995w

Reference yield:

: 142860-83-1
1-(4-methoxybenzyloxy)-3-butene

: 1489365-14-1
N-((3R,10R)-10-((tert-butyldimethylsilyl)oxy)-11-((4-methoxybenzyl)oxy)undec-1-en-3-yl)-4-methoxyaniline

: 1489365-13-0
N-((3S,10R)-10-((tert-butyldimethylsilyl)oxy)-11-((4-methoxybenzyl)oxy)undec-1-en-3-yl)-4-methoxyaniline

Guidance literature:: Multi-step reaction with 5 steps

1.1: palladium diacetate; 4,5-Diazafluoren-9-one / dodecane / 65 °C / Sealed tube

2.1: potassium phosphate; C₄₄H₄₁IrNO₂P / toluene / 25 °C / Glovebox

3.1: 9-borabicyclo[3.3.1]nonane dimer / tetrahydrofuran / 10 h / 20 °C / Glovebox

3.2: polytetrafluoroethylene / 24 h / 20 °C / Sealed tube

4.1: palladium diacetate; 4,5-Diazafluoren-9-one / dodecane / 65 °C / Sealed tube

5.1: potassium phosphate; C₄₄H₄₁IrNO₂P / toluene / 25 °C / Glovebox

With potassium phosphate; 9-borabicyclo[3.3.1]nonane dimer; 4,5-Diazafluoren-9-one; C₄₄H₄₁IrNO₂P; palladium diacetate; In tetrahydrofuran; dodecane; toluene;
DOI:10.1021/ja409995w