methyl 2-{[(benzyloxy)carbonyl]amino}-3-(4-{[(trifluoromethyl)sulfonyl]oxy}phenyl)propanoate

Base Information

Chemical Name:methyl 2-{[(benzyloxy)carbonyl]amino}-3-(4-{[(trifluoromethyl)sulfonyl]oxy}phenyl)propanoate
CAS No.:183021-88-7
Molecular Formula:C₁₉H₁₈F₃NO₇S
Molecular Weight:461.416
Hs Code.:

Synonyms:methyl 2-{[(benzyloxy)carbonyl]amino}-3-(4-{[(trifluoromethyl)sulfonyl]oxy}phenyl)propanoate

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Chemical Property of methyl 2-{[(benzyloxy)carbonyl]amino}-3-(4-{[(trifluoromethyl)sulfonyl]oxy}phenyl)propanoate

Chemical Property:

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Technology Process of methyl 2-{[(benzyloxy)carbonyl]amino}-3-(4-{[(trifluoromethyl)sulfonyl]oxy}phenyl)propanoate

There total 4 articles about methyl 2-{[(benzyloxy)carbonyl]amino}-3-(4-{[(trifluoromethyl)sulfonyl]oxy}phenyl)propanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 37595-74-7
N,N-phenylbistrifluoromethane-sulfonimide

: 13512-31-7
N-(benzyloxycarbonyl)-L-tyrosine methyl ester

: 183021-88-7
methyl 2-{[(benzyloxy)carbonyl]amino}-3-(4-{[(trifluoromethyl)sulfonyl]oxy}phenyl)propanoate

Guidance literature:: With triethylamine; In acetonitrile; at 20 ℃; for 3h; Inert atmosphere;

Reference yield:

: 60-18-4,18875-48-4,25619-78-7,30704-25-7
L-tyrosine

: 183021-88-7
methyl 2-{[(benzyloxy)carbonyl]amino}-3-(4-{[(trifluoromethyl)sulfonyl]oxy}phenyl)propanoate

Guidance literature:: Multi-step reaction with 3 steps

1.1: thionyl chloride / 0.08 h / 0 °C / Inert atmosphere

1.2: 21 h / 0 - 20 °C

2.1: sodium carbonate / water; acetone / 3 h / 20 °C

3.1: triethylamine / acetonitrile / 3 h / 20 °C / Inert atmosphere

With thionyl chloride; sodium carbonate; triethylamine; In water; acetone; acetonitrile;

Reference yield:

: 1080-06-4
L-Tyr-OMe

: 183021-88-7
methyl 2-{[(benzyloxy)carbonyl]amino}-3-(4-{[(trifluoromethyl)sulfonyl]oxy}phenyl)propanoate

Guidance literature:: Multi-step reaction with 2 steps

1: sodium carbonate / water; acetone / 3 h / 20 °C

2: triethylamine / acetonitrile / 3 h / 20 °C / Inert atmosphere

With sodium carbonate; triethylamine; In water; acetone; acetonitrile;