N,N'-bis[6-(4-(diphenylphosphanyl)benzoylamino)pyridin-2-yl]-1,1'-ferrocenedicarboxylic amide

Base Information

Chemical Name:N,N'-bis[6-(4-(diphenylphosphanyl)benzoylamino)pyridin-2-yl]-1,1'-ferrocenedicarboxylic amide
CAS No.:478811-99-3
Molecular Formula:C₆₀H₄₆FeN₆O₄P₂
Molecular Weight:1032.86
Hs Code.:

Synonyms:N,N'-bis[6-(4-(diphenylphosphanyl)benzoylamino)pyridin-2-yl]-1,1'-ferrocenedicarboxylic amide

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Chemical Property of N,N'-bis[6-(4-(diphenylphosphanyl)benzoylamino)pyridin-2-yl]-1,1'-ferrocenedicarboxylic amide

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Technology Process of N,N'-bis[6-(4-(diphenylphosphanyl)benzoylamino)pyridin-2-yl]-1,1'-ferrocenedicarboxylic amide

There total 1 articles about N,N'-bis[6-(4-(diphenylphosphanyl)benzoylamino)pyridin-2-yl]-1,1'-ferrocenedicarboxylic amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 478811-98-2
N,N'-bis[6-(4-iodobenzoylamino)pyridin-2-yl]-1,1'-ferrocenedicarboxylic amide

: 829-85-6
diphenylphosphane

: 478811-99-3
N,N'-bis[6-(4-(diphenylphosphanyl)benzoylamino)pyridin-2-yl]-1,1'-ferrocenedicarboxylic amide

Guidance literature:: With palladium diacetate; triethylamine; In acetonitrile; (Ar); addn. of Et3N, Ph2PH and soln. of Pd(OAc)2 in CH3CN to soln. of Fe(C5H4CONHC5H3NNHCOC6H4I)2 in CH3CN; warming to 85°C in a closed tube ; stirring for 2 h; cooling, pouring into a separatory flask with CH2Cl2; washing of org. phase with satd. soln. of NH4Cl, drying (Na2SO4); evapn. to dryness under vac., chromy., (CH2Cl2/MeOH, 60:1), elem. anal.;
DOI:10.1021/om020364v

Reference yield:

: 478811-99-3
N,N'-bis[6-(4-(diphenylphosphanyl)benzoylamino)pyridin-2-yl]-1,1'-ferrocenedicarboxylic amide

: 32005-36-0
bis(dibenzylideneacetone)-palladium⁽⁰⁾

: [Pd(dba)(N,N'-bis[6-(4-diphenylphosphanyl)benzoylamino)pyridin-2-yl]-1,1'-ferrocenedicarboxylic amide)]

Guidance literature:: In N,N-dimethyl-formamide; (Ar); mixing of Pd(dba)2 and Fe(C5H4CONHC5H3NNHCOC6H4PPh2)2 in DMF; not isolated, monitoring by NMR;
DOI:10.1021/om020364v