[3-(acetyl(tert-butoxycarbonyl)amino)-2,4-dimethylphenyl]tert-butyl carbonate

Base Information

Chemical Name:[3-(acetyl(tert-butoxycarbonyl)amino)-2,4-dimethylphenyl]tert-butyl carbonate
CAS No.:1427407-01-9
Molecular Formula:C₂₀H₂₉NO₆
Molecular Weight:379.453
Hs Code.:

Synonyms:[3-(acetyl(tert-butoxycarbonyl)amino)-2,4-dimethylphenyl]tert-butyl carbonate

Suppliers and Price of [3-(acetyl(tert-butoxycarbonyl)amino)-2,4-dimethylphenyl]tert-butyl carbonate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of [3-(acetyl(tert-butoxycarbonyl)amino)-2,4-dimethylphenyl]tert-butyl carbonate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of [3-(acetyl(tert-butoxycarbonyl)amino)-2,4-dimethylphenyl]tert-butyl carbonate

There total 5 articles about [3-(acetyl(tert-butoxycarbonyl)amino)-2,4-dimethylphenyl]tert-butyl carbonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 24424-99-5
di-tert-butyl dicarbonate

: 100445-95-2
N-(3-hydroxy-2,6-dimethylphenyl)acetamide

: 1427407-01-9
[3-(acetyl(tert-butoxycarbonyl)amino)-2,4-dimethylphenyl]tert-butyl carbonate

Guidance literature:: With dmap; triethylamine; In N,N-dimethyl-formamide; at 50 ℃;

Reference yield:

: 87-62-7
2,6-dimethylaniline

: 1427407-01-9
[3-(acetyl(tert-butoxycarbonyl)amino)-2,4-dimethylphenyl]tert-butyl carbonate

Guidance literature:: Multi-step reaction with 5 steps

1.1: 1 h / 0 - 20 °C

2.1: nitric acid; acetic acid; sulfuric acid / 1 h / 0 - 20 °C

3.1: palladium 10% on activated carbon; hydrogen / ethanol; methanol; acetic acid / 36 h / 20 °C

4.1: sodium nitrite; sulfuric acid / water / 0.5 h / 0 °C

4.2: 2 h / 100 °C

5.1: dmap; triethylamine / N,N-dimethyl-formamide / 50 °C

With dmap; sulfuric acid; palladium 10% on activated carbon; hydrogen; nitric acid; acetic acid; triethylamine; sodium nitrite; In methanol; ethanol; water; acetic acid; N,N-dimethyl-formamide;

Reference yield:

: 2198-53-0
N-(2,6-dimethylphenyl)acetamide

: 1427407-01-9
[3-(acetyl(tert-butoxycarbonyl)amino)-2,4-dimethylphenyl]tert-butyl carbonate

Guidance literature:: Multi-step reaction with 4 steps

1.1: nitric acid; acetic acid; sulfuric acid / 1 h / 0 - 20 °C

2.1: palladium 10% on activated carbon; hydrogen / ethanol; methanol; acetic acid / 36 h / 20 °C

3.1: sodium nitrite; sulfuric acid / water / 0.5 h / 0 °C

3.2: 2 h / 100 °C

4.1: dmap; triethylamine / N,N-dimethyl-formamide / 50 °C

With dmap; sulfuric acid; palladium 10% on activated carbon; hydrogen; nitric acid; acetic acid; triethylamine; sodium nitrite; In methanol; ethanol; water; acetic acid; N,N-dimethyl-formamide;