2-(Phenylthio)ethanethioamide

Base Information

Chemical Name:2-(Phenylthio)ethanethioamide
CAS No.:59865-82-6
Molecular Formula:C8H9 N S2
Molecular Weight:183.298
Hs Code.:
DSSTox Substance ID:DTXSID80381162
Nikkaji Number:J3.238.197I
Wikidata:Q82171821
Mol file:59865-82-6.mol

Synonyms:2-(phenylthio)ethanethioamide;59865-82-6;2-phenylsulfanylethanethioamide;HMS555C07;2-(phenylsulfanyl)ethanethioamide;Maybridge1_004803;2-(Phenylthio)thioacetamide;2-phenylsulfanyl-thioacetamide;SCHEMBL1932674;DTXSID80381162;ZRDOSZLCJHRADP-UHFFFAOYSA-N;MFCD00085154;AKOS006227948;KM 04192;MS-22095;FT-0608906;J-506527

Suppliers and Price of 2-(Phenylthio)ethanethioamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
2-(phenylthio)ethanethioamide
2.5g
$ 240.00

American Custom Chemicals Corporation
2-(PHENYLTHIO)ETHANETHIOAMIDE 95.00%
25G
$ 1893.11

American Custom Chemicals Corporation
2-(PHENYLTHIO)ETHANETHIOAMIDE 95.00%
10G
$ 1512.30

American Custom Chemicals Corporation
2-(PHENYLTHIO)ETHANETHIOAMIDE 95.00%
1G
$ 676.71

Total 7 raw suppliers

Chemical Property of 2-(Phenylthio)ethanethioamide

Chemical Property:

Vapor Pressure:0.000689mmHg at 25°C
Boiling Point:308.2°C at 760 mmHg
Flash Point:140.2°C
Density:1.25g/cm³
XLogP3:1.8
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:3
Exact Mass:183.01764164
Heavy Atom Count:11
Complexity:130

Purity/Quality:

99% ^*data from raw suppliers

2-(phenylthio)ethanethioamide ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)SCC(=S)N

Technology Process of 2-(Phenylthio)ethanethioamide

There total 3 articles about 2-(Phenylthio)ethanethioamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 21.0%

: 22446-20-4
α-(phenylthio)acetamide

: 59865-82-6
2-(phenylthio)ethanethioamide

Guidance literature:: With Lawessons reagent; In toluene; at 80 ℃; for 3.5h; Inert atmosphere;
DOI:10.1002/cmdc.201300414

Reference yield:

: 7031-27-8
(phenylthio)acetic acid chloride

: 59865-82-6
2-(phenylthio)ethanethioamide

Guidance literature:: Multi-step reaction with 2 steps

1: ammonia / tetrahydrofuran; water / 1.5 h / 0 °C

2: Lawessons reagent / toluene / 3.5 h / 80 °C / Inert atmosphere

With Lawessons reagent; ammonia; In tetrahydrofuran; water; toluene;
DOI:10.1002/cmdc.201300414

Reference yield:

: 103-04-8
(phenylthio)acetic acid

: 59865-82-6
2-(phenylthio)ethanethioamide

Guidance literature:: Multi-step reaction with 3 steps

1: oxalyl dichloride; N,N-dimethyl-formamide / tetrahydrofuran / 0.5 h / 0 °C

2: ammonia / tetrahydrofuran; water / 1.5 h / 0 °C

3: Lawessons reagent / toluene / 3.5 h / 80 °C / Inert atmosphere

With Lawessons reagent; oxalyl dichloride; ammonia; N,N-dimethyl-formamide; In tetrahydrofuran; water; toluene;
DOI:10.1002/cmdc.201300414